Preparing method for nickel plating glass fiber fabric/epoxy resin electromagnetic shielding composite material

A technology of glass fiber and epoxy resin, which is applied in the field of preparation of nickel-plated glass fiber fabric/epoxy resin electromagnetic shielding composite materials, which can solve the problems of high price and industrialization of the process.

Inactive Publication Date: 2017-08-22
ZHONGBEI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, most of the electromagnetic shielding materials currently developed use conductive fillers such as carbon nanotubes, metal fibers, and graphene. Although these materials can give full play to their excellent electrical conductivity, expensive prices and sophisticated processes have become excellent products for industrialization. the great shackles of

Method used

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  • Preparing method for nickel plating glass fiber fabric/epoxy resin electromagnetic shielding composite material
  • Preparing method for nickel plating glass fiber fabric/epoxy resin electromagnetic shielding composite material
  • Preparing method for nickel plating glass fiber fabric/epoxy resin electromagnetic shielding composite material

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Embodiment 1 Preparation of nickel-plated glass fiber fabric

[0027] (1) Surface pretreatment of glass fiber fabric:

[0028]Put the glass fiber fabric in the acetone solution, shake it at a constant temperature of 30°C for 20 minutes, and wash it for later use; add the degreased glass fiber fabric into the roughening solution, shake it at a constant temperature of 60°C for 40 minutes, and wash it for later use; Add the glass fiber fabric into the sensitizing solution, shake it at a constant temperature for 20 minutes at 35°C, and wash it for later use; add the sensitized glass fiber fabric into the activation solution, shake it at a constant temperature for 20 minutes at 30°C, and wash it for later use. The composition of the roughening solution is: sodium hydroxide 40g / L; the composition of the sensitization solution is: 30g / L of stannous chloride, 20ml / L of hydrochloric acid of 37wt.%, and the solvent is distilled water; the composition of the activation solution is...

Embodiment 2

[0032] Embodiment 2 Preparation of nickel-plated glass fiber fabric

[0033] (1) Surface pretreatment of glass fiber fabric:

[0034] Put the glass fiber fabric in the acetone solution, shake it at a constant temperature of 30°C for 20 minutes, and wash it for later use; add the degreased glass fiber fabric into the roughening solution, shake it at a constant temperature of 60°C for 40 minutes, and wash it for later use; Add the glass fiber fabric into the sensitizing solution, shake it at a constant temperature for 20 minutes at 35°C, and wash it for later use; add the sensitized glass fiber fabric into the activation solution, shake it at a constant temperature for 20 minutes at 30°C, and wash it for later use.

[0035] The composition of the roughening solution is: sodium hydroxide 40g / L; the composition of the sensitization solution is: 30g / L of stannous chloride, 20ml / L of hydrochloric acid of 37wt.%, and the solvent is distilled water; the composition of the activation s...

Embodiment 3

[0039] Embodiment 3 Preparation of nickel-plated glass fiber fabric

[0040] (1) Surface pretreatment of glass fiber fabric:

[0041] Put the glass fiber fabric in the acetone solution, shake it at a constant temperature of 30°C for 20 minutes, and wash it for later use; add the degreased glass fiber fabric into the roughening solution, shake it at a constant temperature of 60°C for 40 minutes, and wash it for later use; Add the glass fiber fabric into the sensitizing solution, shake it at a constant temperature for 20 minutes at 35°C, and wash it for later use; add the sensitized glass fiber fabric into the activation solution, shake it at a constant temperature for 20 minutes at 30°C, and wash it for later use.

[0042] The composition of the roughening solution is: sodium hydroxide 40g / L; the composition of the sensitization solution is: 30g / L of stannous chloride, 20ml / L of hydrochloric acid of 37wt.%, and the solvent is distilled water; the composition of the activation s...

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Abstract

The invention relates to the field of fiber enhanced resin base functional composite materials, in particular to a nickel plating glass fiber fabric and a method for preparing an epoxy resin electromagnetic shielding composite material with the nickel plating glass fiber fabric as a functional material. Firstly, the glass fiber fabric is subjected to surface pretreatment, so that the surface of the glass fiber fabric has certain catalytic activity. The specific pretreatment technology comprises the steps of oil removing, roughening, sensitization and excitation. Then, the surface of the glass fiber fabric is plated with metal nickel through a chemical plating method. The prepared nickel plating glass fabric is immersed in an epoxy resin base body, and the electromagnetic shielding composite material is prepared through a laminating forming method. Or, the prepared nickel plating glass fiber fabric is laid in the die, and then the epoxy resin electromagnetic shielding composite material is prepared through the RTM forming technology. The volume resistivity of the prepared electromagnetic shielding composite material is 10<-3>omega.cm, the shielding effectiveness can reach 60dB or above within the frequency range of 2-18 GHz, and good mechanical performance is achieved.

Description

technical field [0001] The invention relates to the field of fiber-reinforced resin-based functional composite materials, in particular to a method for preparing a nickel-plated glass fiber fabric / epoxy resin electromagnetic shielding composite material. Background technique [0002] Nickel-plated glass fiber fabric has multiple properties of metal nickel and glass fiber fabric, such as low density, high conductivity, flexibility, corrosion resistance and high mechanical properties, so it not only plays a huge role in the traditional shielding field, And it also has a very broad application prospect in the field of conductive materials. Conductive composite materials and electromagnetic shielding composite materials prepared with metals as conductive fillers cannot be widely used due to the disadvantages of high cost and high density. Therefore, the properties of different materials are organically combined to prepare low-cost, low-density high-conductivity composite materia...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B29C70/34B29C70/48B29C70/54C08L63/00C08K9/02C08K3/08C08K7/14C08J5/08
CPCB29C70/34B29C70/48B29C70/54C08J5/08C08J2363/00C08K3/08C08K7/14C08K9/02C08K2003/0862C08K2201/001C08L63/00
Inventor 刘亚青刘亚楠徐凯白永飞赵贵哲泰钰
Owner ZHONGBEI UNIV
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