Silicon carbon negative electrode material and preparation method thereof
A negative electrode material, silicon carbon technology, applied in the field of silicon carbon negative electrode materials and its preparation, can solve the problems of weak adhesion, affecting the electrochemical performance of silicon carbon materials, etc., and achieve the effect of easy filling
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Embodiment 1
[0040] Embodiment 1, differs from comparative example in that this embodiment comprises the following steps:
[0041] Step 1, preparation of the precursor: the particle size is 100nm elemental silicon, methyl methacrylate, tetraethoxysilane (mass ratio is elemental silicon: methyl methacrylate: tetraethoxysilane=95:4: 1) After NMP is mixed (solid content is 10%) kneading, the revolution is 30 rpm, and the rotation is 300 rpm; kneading for 4 hours to obtain a homogeneously dispersed precursor of elemental silicon, methyl methacrylate, and tetraethoxysilane body;
[0042] Step 2, preparation of worm-like graphene-dominated conductive network structure: select microcrystalline graphite as raw material, then add concentrated sulfuric acid and potassium permanganate for oxidative intercalation, and obtain graphite oxide whose oxygen-containing functional group accounts for 15% of the total mass of graphite oxide. Then heat treatment to obtain worm-like graphene for use;
[0043] ...
Embodiment 2
[0046] Embodiment 2 is different from Embodiment 1 in that this embodiment includes the following steps:
[0047] Step 2, preparation of worm-like graphene-dominated conductive network structure: select microcrystalline graphite as raw material, then add concentrated sulfuric acid and potassium permanganate for oxidative intercalation to obtain graphite oxide whose oxygen-containing functional group accounts for 5% of the entire graphite oxide mass, Then heat treatment to obtain worm-like graphene for use;
[0048] The rest are the same as in Embodiment 1 and will not be repeated here.
Embodiment 3
[0049] Embodiment 3 is different from Embodiment 1 in that this embodiment includes the following steps:
[0050] Step 2, preparation of worm-like graphene-dominated conductive network structure: select microcrystalline graphite as raw material, then add concentrated sulfuric acid and potassium permanganate for oxidative intercalation, and obtain graphite oxide whose oxygen-containing functional group accounts for 20% of the mass of the entire graphite oxide. Then heat treatment to obtain worm-like graphene for use;
[0051] The rest are the same as in Embodiment 1 and will not be repeated here.
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