Device and method for extracting nicotine by using complete equipment of short-range distiller

A short-path distillation and complete set of equipment technology, applied in extractive distillation, tobacco, application and other directions, can solve the problems of low purity and low nicotine yield, and achieve the effect of reducing impurity content and preventing oxidative deterioration.

Inactive Publication Date: 2017-10-03
HUBEI HENO BIOLOGICAL ENG CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to solve the shortcomings of low nicotine yield and low purity in t

Method used

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  • Device and method for extracting nicotine by using complete equipment of short-range distiller
  • Device and method for extracting nicotine by using complete equipment of short-range distiller

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0027] Example 1

[0028] The present invention also provides a method for extracting nicotine using a complete set of short-path distiller equipment, including the following steps:

[0029] S1. The crude nicotine organic solution is pumped by the feed pump 14 to the feed port 15, and then enters the distillation tank 2 for the short-path distillation separation process. The feed temperature of the short-path distiller is 62 ℃, and the heating jacket is used 3 Heat the distillation tank 2 to 63°C, use the vacuum pump 5 to vacuum the distillation tank 2 and control the pressure at 12Pa; in order to improve the extraction rate of refined nicotine products, the distillation tank 2 is lightly assembled The ratio of the sub-to-heavy component is controlled to 2 / 3, and the speed of the film wiper 18 is controlled at 180r / min.

[0030] S2. The final light component refined nicotine product is discharged from the light component outlet 7 into the collection tank 6 for storage.

[0031] The p...

Example Embodiment

[0037] Example 2

[0038] The present invention also provides a method for extracting nicotine using a complete set of short-path distiller equipment, including the following steps:

[0039] S1. The crude nicotine organic solution is pumped from the feed pump 14 to the feed port 15, and then enters the distillation tank 2 for short-path distillation separation process. The feed temperature of the short-path still is 63°C, and the heating jacket is used 3 Heat the distillation tank 2 to 65°C, and use the vacuum pump 5 to vacuum the distillation tank 2 and control the pressure at 13 Pa; in order to increase the extraction rate of refined nicotine products, lighten the distillation tank 2 The ratio of sub-to-heavy component is controlled to 2 / 3, while the speed of the film wiper 18 is controlled at 190r / min.

[0040] S2. The final light component refined nicotine product is discharged from the light component outlet 7 into the collection tank 6 for storage.

[0041] The preparation meth...

Example Embodiment

[0047] Example 3

[0048] The present invention also provides a method for extracting nicotine using a complete set of short-path distiller equipment, including the following steps:

[0049] S1. The crude nicotine organic solution is pumped by the feed pump 14 to the feed port 15, and then enters the distillation tank 2 for short-path distillation separation process, wherein the feed temperature of the short-path still is 65℃, and the heating jacket is used 3 Heat the distillation tank 2 to 68°C, use the vacuum pump 5 to vacuumize the distillation tank 2 and control the pressure at 15Pa; in order to increase the extraction rate of refined nicotine products, lightly combine the distillation tank 2 The ratio of the sub-to-heavy component is controlled to 2 / 3, and the speed of the film wiper 18 is controlled at 200r / min.

[0050] S2. The final light component refined nicotine product is discharged from the light component outlet 7 into the collection tank 6 for storage.

[0051] The pre...

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Abstract

The invention relates to the technical field of nicotine extraction and in particular relates to a device and a method for extracting nicotine by using complete equipment of a short-range distiller. The device comprises a bottom plate, wherein a support rack is fixed on the bottom plate; a distillation tank body is mounted on the support rack; the outer side of the distillation tank body is wrapped with a heating jacket; a motor is connected with the top end of the distillation tank body through a fixing sleeve; the output shaft of the motor is connected with a rotating shaft; a distributor is connected with the upper end of the rotating shaft; membrane scrapers are connected with two sides of the rotating shaft; a condensation circulation pipeline is arranged in the middle inside the distillation tank body; a condenser is connected with the lower end of the condensation circulation pipeline; a feeding hole is formed in one side of the upper end of the distillation tank body; a feeding pump is mounted on one side of the feeding hole; a heavy component outlet is formed in one side of the lower end of the distillation tank body; a light component outlet is formed in the bottom end of the distillation tank body; a vacuum interface is further formed in one side of the lower end of the distillation tank body; and a vacuum pump is connected with the vacuum interface. The invention further provides a method for extracting nicotine by using the complete equipment of the short-range distiller. By adopting the device and the method, the problems of low nicotine yield and purity are solved.

Description

technical field [0001] The invention relates to the technical field of nicotine extraction, in particular to a device and method for extracting nicotine by using a complete set of short-path distillers. Background technique [0002] Natural nicotine, also known as nicotine, is an important medicine, natural pesticide, spice, and chemical raw material. It can be used to produce safe and effective smoking cessation products, electronic cigarettes, and low-toxicity and no residue pesticides. Nicotine with a purity of more than 99.9% is in great demand, and the price at home and abroad is more than 1 million yuan / ton. At present, nicotine is mainly extracted from tobacco or tobacco sticks and tobacco leaves discarded from tobacco production. [0003] Existing nicotine extraction methods such as steam distillation, sulfuric acid stripping, supercritical fluid extraction and ion exchange focus on the extraction rate of nicotine, and mostly use simple distillation methods to refin...

Claims

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Application Information

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IPC IPC(8): B01D3/40A24B15/24
CPCB01D3/40A24B15/243
Inventor 杨强蒲鑫贺择李江刘齐洲
Owner HUBEI HENO BIOLOGICAL ENG CO LTD
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