A kind of nano water-based pigment inkjet ink and preparation method thereof
A water-based pigment, inkjet ink technology, applied in inks, household appliances, applications, etc., to achieve the effects of good ink compatibility, low cost, and good standby performance
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Embodiment 1
[0040] Raw material preparation for a disperse color paste: by weight, weigh PBK7 15%, EFKA4585 15%, ADISPONIL A 1580 2.5%, defoamer Airase5500 0.1%, BASF Joncryl 8055 5% and deionized water 62.4%.
[0041] Preparation method: use Netzsch 6L horizontal nano-sand mill imported from Germany. The cylinder body and tip of the grinder are wear-resistant steel structures. The zirconium beads used are imported zirconium beads with a diameter of 0.25mm. 1300rpm, grind for 18-20h, stop grinding when the particle size of the color paste is 95≤D50≤105nm, D99≤250nm, control the flow rate of the discharge port to 4kg / min, the temperature of the discharge port is 40±2°C, and get nano Grade disperse color paste.
[0042] Test color paste stability
[0043] Centrifuge the color paste at a speed of 10000rpm, filter it with a 1um PP melt-blown filter element imported from PALL, and then take a sample to test the aging stability (thermal stability of the color paste) at 60°C. The aging time is ...
Embodiment 5
[0050] Raw material preparation for a disperse color paste: by weight, PV23 15%, ZetaSperse 3400 15%, DISPONIL A 1580 2.5%, defoamer Airase5500 0.1%, BASF Joncryl 8055 5% and deionized water 62.4%.
[0051] Preparation method: use Netzsch 6L horizontal nano-sand mill imported from Germany. The cylinder body and tip of the grinder are wear-resistant steel structures. The zirconium beads used are imported zirconium beads with a diameter of 0.25mm. 1350rpm, grind for 18-20h, stop grinding when the particle size of the color paste is 95≤D50≤105nm, D99≤250nm, control the flow rate of the discharge port to 3kg / min, the temperature of the discharge port is 38±2°C, and the output will be nano Grade pigment dispersion color paste.
[0052] With the same preparation method as Example 5, different formulations were used to prepare color pastes, namely Examples 6-8 and Comparative Examples 5-8, and the specific formulations are shown in Table 2.
[0053] The color paste formula and perfo...
Embodiment 9
[0058] A kind of raw material preparation of water-based pigment ink-jet ink: by weight, take by weighing 38% of the nano-dispersion color paste of embodiment 1, acrylic resin 15%, glycerol 15%, 1,5-pentanediol 10%, Surfynol 485 0.8%, OP-15 0.5%, Proxel GXL 0.1%, Deionized Water 20.6%.
[0059] Preparation:
[0060] (1) Ink preparation: Turn on the mixer, add deionized water, set the stirring speed to 400rpm, add glycerol, 1,5-pentanediol, Surfynol 485, OP-15, Proxel GXL, stir for 20min until completely dissolved, add 15kg acrylic resin, stir for 20min, set the stirring speed to 600rpm, add 38kg PBK007 nano-pigment dispersion color paste, stir for 40min;
[0061] (2) Aging and filtering: After the preparation is completed, the test viscosity is 6.2, the surface tension is 30, all qualified, and then aged at 30°C for 24 hours, so that the components in the ink are completely dissolved, the dispersion system reaches equilibrium, and the insoluble substances and unstable The co...
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