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Preparation method of novel medical macromolecular material

A polymer material and a new type of technology, applied in the field of preparation of new medical polymer materials, can solve the problems of reduced material modulus, reduced toughness, and thin walls are prone to gaps, etc., and achieve the effects of improving mechanical properties, rigidity and toughness.

Inactive Publication Date: 2017-12-08
南通成山高分子材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, polypropylene also has obvious disadvantages: low impact strength, poor toughness, the toughness is further reduced after adding developer, and the thin wall is prone to cracks or fractures during use.
Conventional polypropylene toughening modification methods such as adding polymer toughening agents can improve the toughness of polypropylene, but the rigidity of polypropylene will be lost, resulting in a sharp decrease in material modulus. It is necessary to add certain reinforcing fillers to polypropylene. Conventional reinforcement Agents such as glass fiber and talc cannot be used due to biosafety and other concerns

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] The preparation method of the novel medical polymer material of the present embodiment, the preparation method comprises the following steps:

[0019] (1) Turn on the plastic high-speed mixer, take 60 parts of polypropylene and 10 parts of styrene-butadiene rubber by weight, and mix at a high speed. The speed of the plastic high-speed mixer is 45r / min, and mix for 40 minutes;

[0020] (2) Put 30 parts of nano-scale light heavy calcium powder and 20 parts of developer into the plastic high-speed mixer, and then perform high-speed mixing at a speed of 45r / min;

[0021] (3) Extrude the uniformly mixed material with twin-screw extrusion. The temperature ranges of twin-screw extrusion are: the temperature of the first zone is 125°C, the temperature of the second zone is 145°C, the temperature of the third zone is 165°C, and the temperature of the fourth zone is 165°C. The temperature is 185°C, and the temperature in the fifth zone is 195°C. After extrusion, it is granulated,...

Embodiment 2

[0023] The preparation method of the novel medical polymer material of the present embodiment, the preparation method comprises the following steps:

[0024] (1) Turn on the plastic high-speed mixer, take 80 parts of polypropylene and 20 parts of styrene-butadiene rubber by weight, and mix at a high speed. The speed of the plastic high-speed mixer is 45r / min, and mix for 40 minutes;

[0025] (2) Put 40 parts of nano-scale light heavy calcium powder and 40 parts of developer into the plastic high-speed mixer, and then perform high-speed mixing at a speed of 45r / min;

[0026] (3) Extrude the uniformly mixed material with twin-screw extrusion. The temperature ranges of twin-screw extrusion are: the temperature of the first zone is 125°C, the temperature of the second zone is 145°C, the temperature of the third zone is 165°C, and the temperature of the fourth zone is 165°C. The temperature is 185°C, and the temperature in the fifth zone is 195°C. After extrusion, it is granulated,...

Embodiment 3

[0028] The preparation method of the novel medical polymer material of the present embodiment, the preparation method comprises the following steps:

[0029] (1) Turn on the plastic high-speed mixer, take 65 parts of polypropylene and 14 parts of styrene-butadiene rubber by weight, and mix at a high speed. The speed of the plastic high-speed mixer is 45r / min, and mix for 40 minutes;

[0030] (2) Put 34 parts of nano-scale light heavy calcium powder and 25 parts of developer into the plastic high-speed mixer, and then perform high-speed mixing at a speed of 45r / min;

[0031] (3) Extrude the uniformly mixed material with twin-screw extrusion. The temperature ranges of twin-screw extrusion are: the temperature of the first zone is 125°C, the temperature of the second zone is 145°C, the temperature of the third zone is 165°C, and the temperature of the fourth zone is 165°C. The temperature is 185°C, and the temperature in the fifth zone is 195°C. After extrusion, it is granulated,...

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PUM

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Abstract

The invention relates to a preparation method of a novel medical macromolecular material. The preparation method comprises the following steps: (1) opening a plastic high-speed mixer to mix 60-80 parts by weight of polypropylene and 10-20 parts by weight of butadiene styrene rubber at a high speed for 40min, wherein the rotating speed of the plastic high-speed mixer is 30-60r / min; (2) then putting 30-40 parts by weight of nanoscale light ground calcium carbonate powder and 20-40 parts by weight of a developing agent into the plastic high-speed mixer to mix at a high speed, wherein the rotating speed is 30-60r / min; and (3) performing twin screw extrusion on the uniformly mixed material, wherein the twin screw extrusion temperature intervals are separately as follows: 120-130 DEG C for a first region, 140-150 DEG C for a second region, 160-170 DEG C for a third region, 180-190 DEG C for a fourth region and 190-200 DEG C for a fifth region; and after extrusion, prilling to obtain the medical macromolecular material. The preparation method disclosed by the invention has the advantages that after adding an additive, some mechanical properties of the macromolecular material can be improved, and the rigidity and toughness of the polypropylene medical macromolecular material are improved.

Description

technical field [0001] The invention belongs to the field of new medical materials, in particular to a preparation method of a novel medical polymer material. Background technique [0002] Medical polymer materials are intended to be directly used on the human body or closely related to human health, so there are strict requirements for materials entering the clinical use stage: [0003] Performance requirements for medical polymer materials: biological aging resistance, stable physical and mechanical properties, easy processing and molding, readily available materials, and reasonable prices. [0004] Requirements for human body effects of medical polymer materials: non-toxic, non-pyrogenic, non-carcinogenic, non-teratogenic, not causing allergic reactions or interfering with the immune mechanism of the body, not destroying adjacent tissues, and not causing calcification on the surface of the material. The contact materials are required to have good blood compatibility and ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/12C08L9/06C08K3/26B29C47/92B29C48/92
CPCC08L23/12B29C48/92B29C2948/92704C08K2003/265C08K2201/011C08L9/06C08K3/26
Inventor 潘征鹏
Owner 南通成山高分子材料有限公司