Active chlorine dioxide disinfectant production method and apparatus

A chlorine dioxide and production method technology, applied in the direction of disinfectants, botany equipment and methods, biocides, etc., can solve the problems of unsatisfactory product quality and cost, difficulty in preparing high-concentration active disinfectants, and increased disinfection costs, etc. problems, to achieve the effect of reducing construction investment and workload, easy operation and less equipment

Active Publication Date: 2017-12-26
SHENZHEN OUTAIHUA ENG EQUIP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The ClO 2 Although the disinfectant solves the problem of storage and transportation, when it is applied, it needs to be activated with a certain concentration of acid to make it re-release ClO 2 Gas, and then sterilize and disinfect, which will inevitably increase the cost of disinfection and the cumbersome operation. Therefore, it is unacceptable to many customers.
On this basis, some manufacturers began to try to produce active ClO 2 Disinfectants, generally use a water injector to absorb ClO at one time 2 The method of gas, due to the poor absorption effect, as a result, the content of the disinfectant can only be a low concentration, fluctuating between 400-800ppm, it is difficult to prepare a high-concentration active disinfectant above 1000ppm, and it is also inconvenient for some applications. Unable to meet customer demand for high-concentration active disinfectants of 2000ppm or above
Some manufacturers also try to use sodium chlorite to prepare a solution, and then activate it to produce a high-concentration active solution. Although this solves the concentration problem, the inherent quality and cost of the product are not ideal, so customers cannot get it. recognition of
[0004] Prior to this, higher concentrations of active ClO 2 Solution production has only been used in industrial pulp bleaching, however, this higher concentration of active ClO 2 The solution is on an industrial generating device and needs to be absorbed under refrigerated water. For this kind of preparation method with large output and high cost, most customers are not suitable and cannot accept it.

Method used

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  • Active chlorine dioxide disinfectant production method and apparatus

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] A kind of production method of active chlorine dioxide disinfectant, comprises the steps:

[0024] (1) The high-purity ClO prepared by the high-purity chlorine dioxide generator 2 The gas is pumped into the middle and upper part of the absorption tank under negative pressure for forced bubbling absorption to make high-concentration active ClO 2 Solution, the finished product is directly sent to the application site through the metering pump;

[0025] (2) The tail gas absorbed by the absorbing tank in step (1) is sucked by the circulating pump through the circulating liquid in the circulating tank, and sucked by the water ejector, and then the exhaust gas absorbed by the circulating tank is passed into the tail gas treatment tank, and the treated intermediate Regular discharge of liquid;

[0026] (3) In step (2), the circulation fluid in the circulation tank overflows into the absorption tank, and the circulation fluid in the circulation tank is supplemented by tap wat...

Embodiment 2

[0029] The difference with embodiment 1 is:

[0030]During normal operation, the high-purity chlorine dioxide generator generates negative pressure through the water ejector suction system, and its negative pressure value is controlled at 8KPa. The absorption tank is under the system negative pressure, and the negative pressure value is controlled at 12KPa. The pressure drop is controlled at 4KPa; the absorption tank absorbs ClO 2 The gas-liquid ratio of the gas is controlled at 1:22; the circulation tank is sucked by the water ejector, and the gas-liquid ratio of the absorbed tail gas is controlled at 4:1.

Embodiment 3

[0032] The high-purity chlorine dioxide generator operates normally under the negative pressure of the system, and the ClO produced 2 Gas, through the water ejector suction system to generate negative pressure, control the negative pressure value of the generator to 7KPa, the absorption tank absorbs ClO under the system negative pressure 2 Gas, the control negative pressure value is 10KPa, the control pressure drop is 3KPa, and the absorption tank absorbs ClO 2 The gas-liquid ratio of the gas is controlled at 1:8, and the active ClO after absorption 2 The disinfectant is directly sent to the application site by the metering pump; after absorption, the exhaust gas is sucked by the water ejector of the circulation tank, and the gas-liquid ratio of the water ejector is controlled to be 2:1.

[0033] Active ClO 2 The result of the test of the finished disinfectant is: ClO 2 Content 2021ppm.

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PUM

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Abstract

The invention discloses an active chlorine dioxide disinfectant production method. The active chlorine dioxide disinfectant production method comprises the following steps: (1) pumping high-purity ClO2 gas prepared by a high-purity chlorine dioxide generator into a middle part and an upper part of an absorption trough under the negative pressure, performing the forced bubbling absorption, preparing a high-concentration active ClO2 solution, and directly sending a finished product into an application field by virtue of a metering pump; (2) absorbing, by the absorption trough, tail gas, enabling circulating liquid of a circulating trough to pass through a circulating pump, pumping by virtue of a water injector, re-introducing the tail gas absorbed by the circulating trough into a tail gas treatment trough, and regularly discharging the treated neutralization solution; and (3) enabling the circulating liquid of the circulating trough to overflow into the absorption trough, and supplementing the circulating liquid of the circulating trough by virtue of tap water. The invention also discloses an apparatus for the method of the invention. By adopting the method, the investment is reduced, the absorption rate is increased, and the effect for absorbing ClO2 is ideal.

Description

technical field [0001] The invention relates to the field of disinfection, in particular to a production method and device of an active chlorine dioxide disinfectant. Background technique [0002] ClO 2 As a new generation of broad-spectrum powerful bactericidal disinfectant recognized internationally, it has been widely used in the disinfection treatment of drinking water, circulating water, sewage, papermaking, air disinfection and civilian products. Due to ClO 2 Rapid sterilization, good effect, no residue, no side effects, so more and more people's approval. [0003] According to ClO 2 Physicochemical properties, its gas is a gas at normal temperature and pressure, and due to its poor stability, resulting in ClO 2 The disadvantages of being unable to store and transport must be prepared and applied now, which brings some inconveniences to the application. With the continuous research and development of preparation technology, and according to the needs of the domest...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N59/00A01N25/02A01P1/00
CPCA01N25/02A01N59/00
Inventor 陈祥衡孙玉石杨温群燕
Owner SHENZHEN OUTAIHUA ENG EQUIP
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