Lithium secondary battery anode and lithium secondary battery including same
A technology of lithium secondary battery and negative electrode, which is applied to the field of negative electrode for lithium secondary battery and lithium secondary battery including the same, can solve the problems of electrolyte loss, loss, battery driving process not continuing, etc.
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preparation example 1
[0124] [Preparation Example 1: Preparation of Negative Electrode]
Embodiment 1
[0126] The Sylgard 184 monomer purchased from Dow Corning is mixed with the hardener in a weight ratio of 10:1 to 10:5. In order to control the thickness to a level of 1 to 10um, hexane was added to dilute the mixture to reduce the concentration. The solution thus prepared is applied on the lithium metal thin film, and then thermally cured at 50 to 100° C. for 1 to 12 hours. At this time, the higher the temperature, the shorter the curing time.
Embodiment 2
[0128] A sol-gel reaction is performed on a single monomer having the following formula 1 to form polysilsesquioxane.
[0129] [Formula 1]
[0130]
[0131] (In Equation 1, R 1 Is oligoethylene glycol)
[0132] The prepared polysilsesquioxane was dissolved in THF in an amount of 10% by weight to obtain a composition for forming a polymer matrix. The composition was applied on a lithium metal thin film as a negative electrode active layer, and then cured at 100°C to form a polymer matrix.
[0133] At this time, the curing time and degree of curing can be shortened by changing the solvent to alcohol or by adding acid or alkali to the solution, in which considering the reactivity of lithium, it can be cured on another substrate such as Teflon sheet or PET sheet The composition is then transferred to a thin lithium film.
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