Synthesis process of polyether polyol serving as ultra-high molecular weight springback agent

An ultra-high molecular weight, polyether polyol technology, applied in the field of textile fabrics, can solve the problems of defect elastic modulus stability, mold release, influence, etc., and achieve the effect of good effect and simple and feasible synthesis process steps.

Pending Publication Date: 2018-02-27
JIANGSU DONGBANG TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, polyether polyols are widely used as ultra-high molecular weight resilience agents, but the defects in their preparation process have affected their elastic modulus stability and mold release properties.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0010] The present invention is further described below:

[0011] A synthesis process of polyether polyol as an ultra-high molecular weight resilience agent, which is characterized in that it comprises the steps of: first adding 80 parts by weight of phthalic anhydride polyester B503 into the kettle, then adding 50 parts by weight of sucrose and 10 parts by weight of propylene glycol, 15 parts by weight of palm oil, 5 parts by weight of soybean oil, and 3 parts by weight of synthetic catalyst C-10; then start stirring and vacuumize, replace with nitrogen two to three times if necessary, heat up to 115° C., and stir for 30 minutes. Then add 1400 parts by weight of propylene oxide in batches of 10-12 times, the temperature of the reaction process should not exceed 125°C, and the pressure in the reactor should not exceed 0.3MPa; pressure; lower the temperature to 105°C, vacuumize (vacuum degree: 0.08-0.1MPa) for 1 hour to remove unreacted propylene oxide and low molecular weight ...

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Abstract

The invention provides a synthesis process of polyether polyol serving as an ultra-high molecular weight springback agent. The synthesis process is characterized by comprising the following steps: adding 80 parts by weight of phenyl anhydride polyester B503 into a kettle; and sequentially adding 50 parts by weight of sucrose, 10 parts by weight of propylene glycol, 15 parts by weight of palm oil,5 parts by weight of soybean oil and 3 parts by weight of a synthesis catalyst C-10. The synthesis process is simple and feasible in steps and good in effect, so that the synthesis process is suitablefor highly elastic materials.

Description

technical field [0001] The invention relates to the field of textile fabrics, in particular to a synthesis process of polyether polyol as an ultra-high molecular weight resilience agent. Background technique [0002] Space suit), especially the extravehicular space suit (Extar Mobility Unit, EMU), is known as the "life talisman" of astronauts. It is a comprehensive protection system made of special materials and has the characteristics of multi-level, multi-module and multi-function. . Aviation suits have evolved from generation to generation. It also showed the concept products of space suits with futuristic colors, which are used for the exploration of the moon and Mars. In addition to functions such as cold protection, shock absorption, radiation resistance, and impact resistance, space suits also need to maintain a constant and stable positive air pressure, which is mainly played by the pressure garment bladder. The mainstream structure of space suits is a multi-layer...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08G63/48C08G65/08
CPCC08G63/48C08G65/08
Inventor 蒋辉宗昀宗伟新
Owner JIANGSU DONGBANG TECH
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