Transparent ceramic material with mechanoluminescence property and preparation method of transparent ceramic material

A transparent ceramic and luminescent technology, which is applied in luminescent materials, chemical instruments and methods, etc., can solve the problems of difficult low-light detection and weak luminous intensity, and achieve high mechanoluminescent efficiency, stable luminescent performance, and high compressive strength Effect

Inactive Publication Date: 2018-04-03
杭州显庆科技有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] In order to overcome a series of problems such as the weak luminous intensity of the mechanoluminescent material in the prior art and the difficulty in low-light detection, the present invention provides a mechanoluminescent transparent ceramic material and a preparation method thereof. High strength, obvious mechanoluminescent effect, etc., can be used for pressure sensing parts in pressure sensors

Method used

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  • Transparent ceramic material with mechanoluminescence property and preparation method of transparent ceramic material
  • Transparent ceramic material with mechanoluminescence property and preparation method of transparent ceramic material
  • Transparent ceramic material with mechanoluminescence property and preparation method of transparent ceramic material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0126] Example 1: The chemical composition is Sr 9.93 Al 5.9 B 0.1 O 19 :0.02Eu 2+ ,0.05Dy 3+

[0127] With high purity SrCO 3 , Al 2 O 3 , H 3 BO 3 , Eu 2 O 3 And Dy 2 O 3 As a raw material, according to the chemical composition of Sr 9.93 Al 5.9 B 0.1 O 19 :0.02Eu 2+ ,0.05Dy 3+ The proportion of each element in the medium, the raw materials are accurately weighed; the agate ball is used as the grinding ball, and the absolute ethanol is used as the ball milling medium. The agate ball, anhydrous ethanol and the raw materials are put into the ball mill tank at the same time, and the ball is mixed on the planetary ball mill. Feed for 5 hours to form a slurry mixture. The mass ratio of anhydrous ethanol to the raw material is 2:3; the obtained slurry mixture is placed in an oven, kept at 80°C for 6 hours, and then dried. The obtained raw materials are passed through a 300-mesh sieve to obtain uniformly mixed raw materials; put the uniformly mixed raw materials into a high-temperature...

Embodiment 2

[0128] Example 2: The chemical composition is Sr 9.92 Al 5.5 B 0.5 O 19 :0.03Eu 2+ ,0.05Gd 3+

[0129] With high purity SrCO 3 , Al 2 O 3 , H 3 BO 3 , Eu 2 O 3 And Gd 2 O 3 As a raw material, according to the chemical composition of Sr 9.92 Al 5.5 B 0.5 O 19 :0.03Eu 2+ ,0.05Gd 3+ The proportion of each element in the medium, the raw materials are accurately weighed; the agate ball is used as the grinding ball, and the absolute ethanol is used as the ball milling medium. The agate ball, anhydrous ethanol and the raw materials are put into the ball mill tank at the same time, and the ball is mixed on the planetary ball mill. Feed for 10 hours to form a slurry mixture. The mass ratio of anhydrous ethanol to the raw material is 2:3; place the obtained slurry mixture in an oven, heat and dry at 70°C for 8 hours, and then dry it. The obtained raw materials are passed through a 300-mesh sieve to obtain uniformly mixed raw materials; put the uniformly mixed raw materials into a high-tempe...

Embodiment 3

[0130] Example 3: The chemical composition is Sr 9.92 Al 5.7 B 0.3 O 19 :0.03Eu 2+ ,0.05Nd 3+

[0131] With high purity SrCO 3 , Al 2 O 3 , H 3 BO 3 , Eu 2 O 3 And Nd 2 O 3 As a raw material, according to the chemical composition of Sr 9.92 Al 5.7 B 0.3 O 19 :0.03Eu 2+ ,0.05Nd 3+ The proportion of each element in the medium, the raw materials are accurately weighed; the agate ball is used as the grinding ball, and the absolute ethanol is used as the ball milling medium. The agate ball, anhydrous ethanol and the raw materials are put into the ball mill tank at the same time, and the ball is mixed on the planetary ball mill. Feed for 15 hours to form a slurry mixture. The mass ratio of anhydrous ethanol to the raw material is 2:3; the obtained slurry mixture is placed in an oven, kept at 75°C for 7 hours, and then dried. The obtained raw materials are passed through a 300-mesh sieve to obtain uniformly mixed raw materials; put the uniformly mixed raw materials into a high-temperatur...

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Abstract

The invention discloses a transparent ceramic material with mechanoluminescence property and a preparation method of the transparent ceramic material, aims to provide a pressure sensing material withthe mechanoluminescence property and belongs to the technical field of the transparent ceramic material. The general formula of chemical composition of the transparent ceramic material is Se(10-y-z)Al(6-x)BxO19:yEu<2+>,zRe<3+>, wherein Re is one or combination of more than one of Dy, Gd and Nd, value ranges of x, y and z are as follows: x is larger than or equal to 0.1 and smaller than or equal to0.5, y is larger than or equal to 0.01 and smaller than or equal to 0.05, and z is larger than or equal to 0.01 and smaller than or equal to 0.05. The luminescence center of the transparent ceramic material is Eu<2+> ions, and the mechanoluminescence effect of the transparent ceramic material can be effectively enhanced by introducing rare earth impurity ions such as Dy<3+>, Gd<3+> and Nd<3+>. The transparent ceramic material has the characteristics of high compressive strength, remarkable mechanoluminescence effect and the like and can be applied to pressure sensing components in pressure sensors.

Description

Technical field [0001] The invention belongs to the technical field of transparent ceramic materials, and particularly relates to a force-induced luminescence transparent ceramic material and a preparation method thereof. Background technique [0002] With the rapid development of information processing and intelligent technology, the sensor is becoming more and more important as the front-end unit of the information acquisition system and has become a key component of the intelligent system. In various industrial control processes, pressure is one of the important parameters in production. Pressure sensor is a special device used to detect and monitor the pressure of system components. It is widely used in building structures, mechanical equipment, aircraft and vehicles, etc. Various areas of the national economy and people’s lives. The existing various pressure sensitive components usually convert the measured pressure signal into an easy-to-measure electrical signal for outpu...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/01C04B35/622C09K11/77
CPCC04B35/01C04B35/622C04B2235/3217C04B2235/3224C04B2235/3409C04B2235/6562C04B2235/6567C04B2235/658C04B2235/662C04B2235/9653C09K11/774
Inventor 杨道救
Owner 杭州显庆科技有限公司
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