A method for the discharge of triazone pesticide wastewater up to the standard and coordinated with the treatment of salt resources
A technology for pesticide wastewater and triazinone, which is applied in the fields of natural water treatment, water/sewage treatment, chemical instruments and methods, etc., can solve the problem of low comprehensive degradation rate of triazinone pesticide wastewater treatment.
Active Publication Date: 2019-02-26
江苏南大华兴环保科技股份公司
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[0007] Aiming at the problem that the comprehensive degradation rate of triazinone pesticide wastewater treatment is not high in the prior art, the present invention provides a method for triazinone pesticide wastewater to be discharged up to the standard and coordinated with salt resource treatment, which realizes the treatment of triazone pesticide wastewater up to the standard, At the same time, the refined industrial sodium chloride is recovered, which reduces the treatment cost of triazinone pesticide wastewater
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Embodiment 1
[0035] combine figure 1 From the point of view, the present embodiment proposes a method for the discharge of triazinone pesticide wastewater up to standard and coordinated salt resource treatment (wherein the triazinone pesticide wastewater is the triazone pesticide wastewater in the first workshop of a certain pesticide enterprise in Binhai, Jiangsu, and its Basic properties are shown in table 1), and its steps are as follows:
[0036] (1) After the intermediate dichloropinatone production section wastewater in the triazinone pesticide preparation process in the workshop is collected separately to the collection pool (the relevant indicators of the intermediate dichloropinatone production section wastewater are shown in Table 1), collect The intermediate dichloropinatone production section waste water is pumped into the iron-carbon micro-electrolysis kettle, and then in the pH condition of the intermediate dichloropinatone production section waste water (the control pH value...
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Abstract
The invention discloses a triazone pesticide wastewater up-to-standard emission synergistic salt recycling treatment method and belongs to the technical field of pesticide wastewater treatment. The method comprises the following steps: separately collecting and treating wastewater of a triazone pesticide preparation process, performing combined treatment of microelectrolysis-Fenton oxidation-neutralization and sedimentation treatment and UASB (Upflow Anaerobic Sludge Blanket) and aerobiotic activity sludge on wastewater of an intermittent dichloropinacolin production section, performing resinadsorption treatment on wastewater of a triazone production section, recycling sodium chloride, finally combining effluents of the two modes, and accessing to a garden tube network for garden management. By adopting the triazone pesticide wastewater up-to-standard emission synergistic salt recycling treatment method disclosed by the invention, efficient and stable treatment on high-salt, high-COD(Chemical Oxygen Demand) and biorefractory wastewater is achieved, and the purpose of up-to-standard emission of triazone pesticide wastewater is achieved; the method is simple and convenient to operate and has the advantages of high efficiency, low consumption, high stability, convenience of maintenance, and the like, and sodium chloride in the wastewater can be recycled and reused.
Description
technical field [0001] The invention belongs to the field of pesticide wastewater treatment technology, and in particular relates to a method for the discharge of triazinone pesticide wastewater up to the standard and cooperative salt resource treatment. Background technique [0002] Triazone compounds are a class of nitrogen-containing heterocyclic compounds with potential biological activity, wherein triazone (chemical name 6-tert-butyl-4-amino-3-mercapto-1,2,4-triazine-5 (4H)-ketone) is an important intermediate for the synthesis of the herbicide mecinazone. It mainly synthesizes the intermediate of dichloropinatone through the chlorination of pinazone. The intermediate of dichloropinatone undergoes hydrolysis, oxidation, and cyclization. The synthesis of triazone will produce a large amount of high-COD, high-salt, and biologically toxic wastewater during its production process. The wastewater produced by the intermediate dichloropinazone production section is mainly poll...
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IPC IPC(8): C02F9/14C01D3/06C02F101/12C02F101/30C02F101/38C02F103/34
CPCC01D3/06C02F1/041C02F1/285C02F1/461C02F1/66C02F1/72C02F1/725C02F1/78C02F3/30C02F9/00C02F2001/007C02F2101/12C02F2101/306C02F2101/38C02F2101/40C02F2103/343
Inventor 戴建军赵选英杨峰李正斌刘莉莉陈利芳杜虎
Owner 江苏南大华兴环保科技股份公司
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