Preparation method of functional microcapsule
A microcapsule and functional technology, applied in the field of functional microcapsule preparation, can solve the problems of odor generation, insufficient efficacy, poor antibacterial and odor removal effects, etc., and achieve the effect of improving comfort.
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Embodiment 1
[0028] This embodiment provides a method for preparing functional microcapsules, comprising the following steps:
[0029] Including the following steps:
[0030] (1) prepare antibacterial agent, with vetiver root extract, Platycodon grandiflora extract, multi-stem almanus extract, clove flower extract, garlic extract, nano-silver powder, methyl glucose dioleate and Deionized water is mixed and stirred according to a predetermined ratio to obtain an antibacterial agent;
[0031] (2) shellac, gelatin, water and β-cyclodextrin are mixed according to a predetermined ratio to obtain a mixture, and the antibacterial agent is used as a core material, and the mixture is used as a wall material to prepare microcapsules by a dry spraying method.
[0032] Specifically, the method for obtaining the mixture in step 2 is to mix 0.7 parts by mass of shellac, 0.6 parts by mass of gelatin and 12 parts by mass of water at a temperature of 40°C and stir at a speed of 60 rpm The first mixture w...
Embodiment 2
[0036] As a specific scheme of Example 1, the specific method for preparing the antibacterial agent in the step (1) is to mix the root extract of vetiver and the extract of Platycodon grandiflorum according to a predetermined ratio, and mix them at a temperature of 10-30° C. at a temperature of 200-250 Stir at a stirring rate of rpm for 30-40min, then raise the temperature to 60°C at a rate of 10°C / min, and maintain it for 10-20 minutes, and obtain the third mixture after cooling to room temperature;
[0037] Mix the extract of Almanes multistemma, clove flower extract and deionized water and stir at a temperature of 30-50°C at a speed of 150-200 rpm for 5-10min, and obtain the fourth The mixture, the third mixture, the fourth mixture and the garlic extract are mixed at a temperature of 5-10°C and stirred at a speed of 80-120 rpm for 10-15min to obtain the fifth mixture, at a temperature of 5-10°C Next, add nano-silver powder and methyl glucose dioleate to the fifth mixture, a...
Embodiment 3
[0039] As a specific scheme of Example 1, it also includes adding an emulsifier and a dispersant to the mixture, and the emulsifier includes inulin lauryl carbamate, sodium cocoyl glycinate, sodium laurate, hemelonium chloride or cocoyl Glucoside.
[0040] Specifically, the upper dispersant is sodium polyacrylate, acrylic acid or maleic acid cinder copolymer.
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