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A kind of high and low temperature instrument oil composition and preparation method thereof

A kind of instrument oil, high and low temperature technology, applied in the direction of lubricating composition, petroleum industry, etc., to achieve the effect of wide service temperature range, excellent anti-wear and anti-friction and anti-scattering properties, good material compatibility

Active Publication Date: 2020-11-17
武汉博达特种润滑技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For high and low temperature instrument oils with a wider temperature range of -70°C to +150°C, there are no domestic and foreign literature reports

Method used

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  • A kind of high and low temperature instrument oil composition and preparation method thereof
  • A kind of high and low temperature instrument oil composition and preparation method thereof
  • A kind of high and low temperature instrument oil composition and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0056] 1) 89.35 kg of ethyl silicone oil (V 50 =16.85mm 2 / s) and 10 kg of bis(2-ethylhexyl) sebacate were added to the reaction kettle, heated and stirred to 110±5°C, vacuumed to -0.05MPa, and kept at constant temperature and constant vacuum for 60±5 minutes for dehydration ;

[0057] 2) Add 0.3 kg of 2,6-di-tert-butyl-p-cresol, 0.1 kg of N-phenyl-α-naphthylamine, 0.2 kg of dodecenylsuccinic acid and 0.05 kg of benzotriazole , stirred for 15±5 minutes, then cooled to 60±5°C;

[0058] 3) Filter twice through a bag filter with a precision of 1 μm to obtain high and low temperature instrument oil.

Embodiment 2

[0060] 1) 94.4 kg of ethyl silicone oil (V 50 =13.73mm 2 / s) and 5 kg of bis(2-ethylhexyl) adipate were added to the reaction kettle together, heated and stirred to 110±5°C, vacuumed to -0.05MPa, and kept at constant temperature and constant vacuum for 45±5 minutes for dehydration ;

[0061] 2) Add 0.1 kg of 2,6-di-tert-butyl-p-cresol, 0.2 kg of N-phenyl-β-naphthylamine, 0.2 kg of sorbitan monooleate and 0.1 kg of benzotriazepam Azole derivatives, stirred for 15±5 minutes, then cooled to 60±5°C;

[0062] 3) Filter twice through a bag filter with a precision of 1 μm to obtain high and low temperature instrument oil.

Embodiment 3

[0064] 1) 148.2 kg of ethyl silicone oil (V 50 =20.21mm 2 / s) and 50 kg of bis(2-ethylhexyl) sebacate were added to the reaction kettle together, heated and stirred to 120°C±5°C, vacuumed to -0.05MPa, and kept at constant temperature and constant vacuum for dehydration at 60±5 minute;

[0065] 2) sequentially add 0.4 kg of 4,4'-methyl bisphenol, 0.7 kg of octylbutyl diphenylamine, 0.2 kg of dodecenyl succinic acid and 0.2 kg of sorbitan monooleate, 0.1 Kg of benzotriazole and 0.2 kg of 2,5-dithio-1,3,4-thiadiazole derivatives, stirred for 15±5 minutes, then cooled to 60±5°C;

[0066] 3) Filter twice through a bag filter with a precision of 1 μm to obtain high and low temperature instrument oil.

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Abstract

The invention discloses a high-low temperature instrument oil composition. The high-low temperature instrument oil composition comprises, by mass, 56.8-94.78%of ethyl silicone oil, 5-40% of diester base oil, 0.1-2% of an antioxidant, 0.1-1% of an anti-rust agent and 0.02-0.2% of metal deactivator. The invention also discloses a preparation method of the high-low temperature instrument oil composition. The high-low temperature instrument oil has excellent low temperature performances, and can be used in -70 DEG C extremely cold regions or in the sky, and the low temperature of the high-low temperature instrument oil is about 10 DEG C lower than the low temperature of instrument oils in the prior art. The high-low temperature instrument oil also has the advantages of good high temperature property, good lubricity, good protection property and extremely long service life. The high-low temperature instrument oil can be applied to various aerospace and aviation instrument bearings, miniature motor bearings, actuator gears, and precision instruments used in the extremely cold regions.

Description

technical field [0001] The invention relates to an instrument oil and a preparation method thereof, in particular to a high-low temperature instrument oil composition and a preparation method thereof. Background technique [0002] Meters are widely used in various industrial fields as instruments for counting, measuring, timing and other functions. It has the characteristics of small size, high precision, low load, wide working temperature range and long service life. [0003] In order to meet the precise work of the instrument, there are the following requirements for the instrument oil: [0004] 1) Excellent wear resistance and low friction coefficient, can provide good lubrication for the bearing and transmission mechanism of the instrument; [0005] 2) Excellent high-temperature stability and viscosity-temperature properties, extremely low pour point, and low starting torque at low temperature, ensuring that the instrument can work normally at various temperatures; ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10M169/04C10N40/06C10N40/02C10N40/04C10N30/08C10N30/06C10N30/10C10N30/12
CPCC10M169/044C10M2207/024C10M2207/026C10M2207/046C10M2207/123C10M2207/2825C10M2215/064C10M2215/065C10M2215/223C10M2219/106C10M2229/041C10N2030/06C10N2030/08C10N2030/10C10N2030/12C10N2040/02C10N2040/04C10N2040/06
Inventor 曹杰
Owner 武汉博达特种润滑技术有限公司