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Compound synthetic fatliquor and preparation method thereof

A kind of fatliquoring agent and compound type technology, which is applied in the field of compound synthetic fatliquor and its preparation, can solve the problems of single performance and few types of synthetic fatliquor

Inactive Publication Date: 2018-06-26
QINGDAO XIANGZHI ELECTRONICS TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But at present, there are few types of synthetic fatliquor, single performance, and most of them are low and mid-range fatliquor mainly based on natural oil and its modified products

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Add 100g of C16-18 alcohol into a four-necked glass flask equipped with a stirrer, a thermometer and a condenser, raise the temperature to 75°C, add 25g of maleic anhydride after melting, and react for 2.5 hours to obtain C16-18 alcohol succinate, then 100 g of sodium sulfite solution was added dropwise therein, and the reaction was incubated for 5 hours to obtain C16-18 alcohol sulfosuccinate. Cool down to 50°C, then add 120g of 10# white oil, 20g of simethicone oil with a viscosity of 500cp, 75g of sulfited lanolin, and 35g of emulsifier, stir well for 1 to 2 hours, then add triethanolamine for neutralization, Adjust the pH of the system to 7.5-8.5 by adding water to adjust the water content≦50%, then add 6g of isobutanol and continue stirring for 1 hour to obtain about 957 grams of compound synthetic fatliquoring agent.

Embodiment 2

[0024] Add 100g of C16-18 alcohol into a four-necked glass flask equipped with a stirrer, a thermometer and a condenser, heat up to 75°C, add 27g of maleic anhydride after melting, and react for 3 hours to obtain C16-18 alcohol succinate, then 105 g of sodium metabisulfite solution was added dropwise thereto, and the reaction was incubated for 4 hours to obtain C16-18 alcohol sulfosuccinate. Cool down to 50°C, then add 100g of 10# white oil, 16g of simethicone oil with a viscosity of 1000cp, 80g of sulfited lanolin, and 36g of emulsifier, stir well for 1 to 2 hours, then add 30% liquid subtraction to carry out Neutralize, adjust the pH of the system to 7.5-8.5, add water, adjust the water content to 50%, then add 5g of isopropanol and continue stirring for 1 hour to obtain about 933 grams of compound synthetic fatliquoring agent.

Embodiment 3

[0026] Add 100g of C20 alcohol into a four-necked glass flask equipped with a stirrer, a thermometer and a condenser, raise the temperature to 75°C, add 21g of maleic anhydride after melting, and react for 3 hours to obtain C20 alcohol succinate, and then add it dropwise 100g of sodium metabisulfite solution was incubated for 5 hours to obtain C20 alcohol sulfosuccinate. Cool down to 50°C, then add 100g of 5# white oil, 18g of simethicone oil with a viscosity of 100cp, 70g of sulfited lanolin, and 37g of emulsifier, stir well for 1 to 2 hours, then add ethanolamine for neutralization, adjust The pH value of the system is 7.5-8.5, add water to adjust the water content≦50%, then add 6g of isobutanol and continue stirring for 1 hour to obtain about 898 grams of compound synthetic fatliquoring agent.

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Abstract

The invention provides a kind of compound synthetic fatliquor and a preparation method thereof. The compound synthetic fatliquor comprises high-carbon-alcohol disodium laureth sulfosuccinate, mineraloil, silicon oil, sulfited lanoline, an emulsifying agent and a stabilizing agent. The performance of leather can be improved through the compound synthetic fatliquor. The preparation method of the compound synthetic fatliquor comprises the following steps of (1) dripping a sulfonating agent solution to the high-carbon-alcohol disodium laureth sulfosuccinate to have a reaction at 70-100 DEG C for4-10 h; (2) cooling the solution to 50 DEG C, adding the mineral oil, the silicon oil, the sulfited lanoline and the emulsifying agent, conducting stirring for 1-2 h, adding alkali to conduct neutralization and adjusting the pH value to 7.5-8.5; and (3) adding a certain amount of water into the solution, adding the stabilizing agent again and conducting stirring to obtain the compound synthetic fatliquor. The preparation method is relatively simple and has low requirements for equipment, and the production cycle is short.

Description

technical field [0001] The present invention relates to a kind of fatliquoring agent and its preparation method, more specifically, the present invention relates to a kind of composite synthetic fatliquoring agent and its preparation method. Background technique [0002] Fatliquor is the most used leather chemical material in leather production, and it is also one of the important chemical materials in leather processing. It can not only lubricate the leather fiber, prevent the leather from being stiff and cracking, but also make the leather have corresponding toughness and softness, and maintain its strength. It can be said that fatliquor is one of the important factors affecting the quality and performance of leather. In the tanning industry, synthetic fatliquor has been valued and favored by people for its excellent fatliquoring effect, and its type and quantity are also increasing year by year, and it has always been a high-grade fatliquoring agent. The molecular struct...

Claims

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Application Information

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IPC IPC(8): C14C9/02
CPCC14C9/02
Inventor 李辉
Owner QINGDAO XIANGZHI ELECTRONICS TECH CO LTD
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