Uniform heating type spiral plate fixed bed reactor for gas-solid catalytic reaction
A fixed-bed reactor and fixed-bed reaction technology, applied in chemical instruments and methods, preparation of organic compounds, organic chemistry, etc., can solve the problem of poor heat transfer effect, low utilization rate of catalyst bed space, and difficulty in large-scale devices, etc. problem, to achieve the effect of not easy to foul and block, high production capacity, large volume utilization rate
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Embodiment 1
[0030] 150,000 tons / year dimethyl oxalate (DMO) hydrogenation reactor
[0031] When the reactor of the present invention is used as a 150,000-ton / year DMO hydrogenation reactor, 8 sections of spiral plate reaction sections are required after calculation, and its structure is shown in image 3 and Figure 4 . The heat exchange medium inlet 1 is set on the top side of the reactor, and the outlet 2 is set on the upper side of the reactor. The gas enters the reactor from the top air inlet 3, passes through the catalyst fixed bed (8-15) to react, and leaves the reactor together with the product through the bottom gas outlet 4; the heat exchange medium passes through the annular pipe distributor 5 at the top of the reactor , distributed in proportion to the outer inlet of each spiral plate reaction section (08-15) by a number of distribution pipes 6, the heat is exchanged by the heat exchange medium channel spirally, and after the central pipe 7 entering the center of the reaction...
Embodiment 2
[0037] 35,000 tons / year vinyl acetate synthesis reactor
[0038] When the reactor of the present invention is used as a 35,000-ton / year vinyl acetate synthesis reactor, 10 sections of spiral plate reaction sections are needed after accounting, and its structure is shown in Figure 5 and Figure 6 . In order to further enhance the heat exchange effect, a heat exchange medium is installed in each spiral plate reaction section to realize segmental temperature control, specifically: the heat exchange medium inlets 2 and 5-1 (medium temperatures can be the same or different) are set at The lower part of the spiral plate reaction section is connected to the outside of the heat exchange medium channel inside the reaction section. The heat exchange medium is spirally exchanged by the heat exchange medium channel. After entering the central tube 6-1 in the center of the reaction section, it flows out from the heat exchange medium outlet 1. The gas enters the reactor through the top g...
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