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A brush calligraphy ink correction fluid and preparation method thereof

A technology of correction fluid and calligraphy, which is applied in the direction of coating, etc., can solve the problems of calligraphy writing, error correction, ink marks, pollution, etc., and achieve the effects of reducing paper consumption, high coating efficiency, and ensuring uniformity and fullness

Active Publication Date: 2021-03-30
SHANXI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to provide a brush calligraphy ink correction fluid and its preparation method in order to solve the problems of error correction and ink pollution in calligraphy writing

Method used

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  • A brush calligraphy ink correction fluid and preparation method thereof
  • A brush calligraphy ink correction fluid and preparation method thereof
  • A brush calligraphy ink correction fluid and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] A brush calligraphic ink in this embodiment is applied, composed of the following mass percentage of raw materials:

[0024]

[0025]

[0026] The silica coated titanium dioxide nanoma is prepared from the following steps:

[0027] (1) TIO 2 Surface hydroxylation treatment: 100 mg TiO under magnetic stirring 2 P 25 The powder was added to a NaOH solution of 10 ml of a concentration of 0.5 mol / L, and stirred for 9 h, then washed with deionized water to dispersion to dispersion, it is weak to acid, to obtain TiO of surface hydroxylation treatment 2 nanomaterials;

[0028] (2) TiO of hydroxylated surface obtained by step (1) 2 The nanomaterials were dispersed into 30 ml of anhydrous ethanol, and the ultrasound was oscillated for 15 minutes to make it sufficiently dispersed, prepared for TiO 2 Nanomaterial dispersion;

[0029] (3) Ethyl orthosilicate and a mass concentration of 28% ammonia water and anhydrous ethanol are fully mixed by a volume ratio of 1: 1.1: 1, and pre...

Embodiment 2

[0034] A brush calligraphic ink in this embodiment is applied, composed of the following mass percentage of raw materials:

[0035]

[0036] The silica coated titanium dioxide nanoma is prepared from the following steps:

[0037] (1) TIO 2 Surface hydroxylation treatment: under magnetic stirring conditions, 200 mg TiO 2 P 25 The powder was added to a NaOH solution of 10 ml of 1 mol / L, and the stirring was held for 12 h, then the dispersion was washed with deionized water to the dispersion, which was weakly acidic to obtain a surface hydroxylated TiO. 2 nanomaterials;

[0038] (2) TiO of hydroxylated surface obtained by step (1) 2 The nanomaterial is dispersed into 50 mL of anhydrous ethanol, and the ultrasonic oscillation of 30 min makes it sufficiently dispersed, prepared to get TiO 2 Nanomaterial dispersion;

[0039] (3) Ethyl lysate and the mass concentration of 28% ammonia water and anhydrous ethanol are thoroughly mixed by a volume ratio of 1: 2: 2, and prepared a mixed d...

Embodiment 3

[0044] A brush calligraphic ink in this embodiment is applied, composed of the following mass percentage of raw materials:

[0045]

[0046] The silica coated titanium dioxide nanoma is prepared from the following steps:

[0047] (1) TIO 2 Surface hydroxylation treatment: under magnetic stirring conditions, 400 mg TiO2 P 25 The powder was added to a NaOH solution of 10 ml of 2 mol / L, and was allowed to be stirred for 15 h, and then washed with deionized water to centrifugally, the dispersion was weak, resulting in surface hydroxylation treatment TiO 2 nanomaterials;

[0048] (2) TiO of hydroxylated surface obtained by step (1) 2 Nanofilm material is dispersed into 80 mL of anhydrous ethanol, and the ultrasound oscillate 50min makes it fully dispersed, preparing TiO 2 Nanomaterial dispersion;

[0049] (3) Ethyl n-silicate and a mass concentration of 28% ammonia water and anhydrous ethanol are mixed in a volume ratio of 1: 3.5: 4, and the mixed dispersion is prepared.

[0050] (...

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Abstract

The invention relates to a brush calligraphy ink correcting fluid and a preparation method thereof, and aims to solve the problems caused by error correction and ink pollution in brush writing. The invention adopts a technical scheme as follows: the brush calligraphy ink correcting fluid comprises the following raw materials in percent by mass: 40-60% of a silicon dioxide-coated titanium dioxide nanomaterial, 10-20% of chlorinated polyethylene, 5-10% of absolute ethanol, 4-8% of glycerin and the balance of deionized water. The preparation method comprises the following steps: adding the deionized water into a preparation kettle, heating to 40-60 DEG C, adding the glycerin and the absolute ethanol while stirring, then slowly adding a chlorinated polyethylene emulsion, and uniformly stirring; then adding the silicon dioxide-coated titanium dioxide nanomaterial, and stirring for 1.5-3h under a 40-60 DEG C condition. Through the introduction of the silicon dioxide-coated titanium dioxide nanomaterial as a coating main body pigment into the brush calligraphy ink correcting fluid, the dispersion stability of the brush calligraphy ink correcting fluid and the adhesion of a improve layer are improved, the thickness of the coating layer is effectively reduced, and an aesthetic property and the timeliness of a calligraphy work are guaranteed.

Description

Technical field [0001] The present invention relates to a brush calligraphic ink coating and preparation method thereof. Background technique [0002] With the proposal of national cultural construction, traditional cultural education has been greatly attached to, and the brush calligraphy will also get more and more popular in education. The development of brush calligraphy education will inevitably consume a large number of related items such as ink, pen, paper and, and inappropriate use processes will bring great environmental issues and economic burdens. For example, in the brush calligraphy practice or writing process, it will inevitably have problems with writing handwriting and ink pollution paper. Traditional methods will lose their original paper to change paper for continuing writing, which will cause great economic waste and environmental burden; For example, for a long written calligraphy writing, in order to pursue the integrity and aesthetics of the work, an acciden...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D10/00
CPCC09D10/00
Inventor 刘雪峰芦冬涛周叶红马学文双少敏董川
Owner SHANXI UNIV
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