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Low-viscosity calcined kaolin, low-viscosity calcined kaolin slurry and preparation method thereof

A technology of calcined kaolin and low viscosity, which is applied in the direction of fibrous filler, dyed polymer organic compound treatment, coating, etc. It can solve the problems that affect the application range of calcined kaolin and the viscosity of the slurry, and achieve good practicability and reaction conditions Mild, easy-to-prepare effects

Active Publication Date: 2020-11-10
内蒙古超牌新材料股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The invention provides a low-viscosity calcined kaolin, a low-viscosity calcined kaolin slurry and a preparation method thereof to solve the technical problem that the high-concentration calcined kaolin slurry has a high viscosity and affects the application range of the calcined kaolin

Method used

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Examples

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preparation example Construction

[0033] In the preparation method of the above-mentioned low-viscosity calcined kaolin, the polyvinyl alcohol solution is directly added to the slurry of the calcined kaolin, and after drying, the low-viscosity calcined kaolin is obtained. If the polyvinyl alcohol solution is only added when preparing the calcined kaolin slurry, the viscosity of the calcined kaolin slurry cannot be significantly reduced. The invention has simple preparation process, mild reaction conditions, good repeatability and is suitable for large-scale production. The prepared low-viscosity calcined kaolin has been tested, simulated and applied in production, and the effect is remarkable and the practicability is good.

[0034]Preferably, the mass concentration of the calcined kaolin slurry is 20-55%. Usually, calcined kaolin and water are mixed in a weight ratio of 1-3:1. When the mass concentration of calcined kaolin slurry reaches more than 55%, the higher the concentration, the faster the viscosity w...

Embodiment 1

[0047] The low-viscosity calcined kaolin in this embodiment includes calcined kaolin and polyvinyl alcohol adsorbed on the surface of the calcined kaolin, and the polyvinyl alcohol is 0.3% of the mass of the calcined kaolin. Calcined kaolin: average particle size 0.9μm; polyvinyl alcohol specification: 17-99.

[0048] The preparation method of the low-viscosity calcined kaolin of the present embodiment:

[0049] Dissolve polyvinyl alcohol in hot water at 98°C in advance, stir for 20 minutes, and prepare a solution with a mass concentration of 2%. The calcined kaolin is prepared into a slurry with a mass concentration of 40%, sodium hexametaphosphate is added as a dispersant, and the sodium hexametaphosphate is 0.3% by mass of the calcined kaolin. Add the above-prepared polyvinyl alcohol solution into the calcined kaolin slurry in an amount of 0.3% of the mass of the calcined kaolin. The calcined kaolin slurry containing polyvinyl alcohol is dried in a spray dryer, and then d...

Embodiment 2

[0053] The low-viscosity calcined kaolin in this embodiment includes calcined kaolin and polyvinyl alcohol adsorbed on the surface of the calcined kaolin, and the polyvinyl alcohol is 0.05% of the mass of the calcined kaolin. Calcined kaolin: average particle size 0.9μm; polyvinyl alcohol specification: 17-88.

[0054] The method for preparing low-viscosity calcined kaolin in this embodiment.

[0055] Dissolve polyvinyl alcohol in hot water at 98°C in advance, stir for 20 minutes, and prepare a solution with a mass concentration of 2%. The calcined kaolin is formulated into a slurry with a mass concentration of 50%, and sodium polyacrylate is added as a dispersant, and the sodium polyacrylate is 0.3% of the mass of the calcined kaolin. The polyvinyl alcohol solution prepared above is added to the calcined kaolin slurry in an amount of 0.05% of the mass of the calcined kaolin. The calcined kaolin slurry containing polyvinyl alcohol is dried in a spray dryer, and then disperse...

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Abstract

The invention discloses low-viscosity calcined kaolin, low-viscosity calcined kaolin slurry and a preparation method thereof, wherein the low-viscosity calcined kaolin comprises calcined kaolin and polyvinyl alcohol which is adsorbed on the surface of the calcined kaolin; and the polyvinyl alcohol is 0.05 to 1 percent of the mass of the calcined kaolin. Calcined kaolin particles are coated with the polyvinyl alcohol, so that the affinity between the low-viscosity calcined kaolin particles and water molecules is improved and the viscosity of the low-viscosity calcined kaolin particles slurry isreduced. The application range of the low-viscosity calcined kaolin is enlarged.

Description

technical field [0001] The invention relates to the field of kaolin preparation, in particular to a low-viscosity calcined kaolin. In addition, the invention also relates to a low-viscosity calcined kaolin slurry and a preparation method thereof. Background technique [0002] Calcined kaolin is made of kaolin as raw material and calcined at high temperature to change the chemical properties of the material to meet certain requirements. The particle size of ultrafine calcined kaolin is less than 1 μm. In water-based systems such as coatings, ultra-fine calcined kaolin has higher hiding power and viscosity than 1250 mesh calcined kaolin products with a coarser particle size. However, when it is desired to prepare calcined kaolin slurry with a higher concentration to meet certain industrial needs, ultrafine calcined kaolin is difficult to meet the application requirements because of its high viscosity. Surface modification treatment is a common technical means to improve the...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09C1/42C09C3/10C09D7/62
CPCC01P2006/22C09C1/42C09C3/10C09D7/62
Inventor 冯建明林炼王宇轩陈建文刘世明张娜
Owner 内蒙古超牌新材料股份有限公司