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Detection device for migration quantity of phthalate ester compound and tributyl phosphate for special filter tip and detection method of detection device

A technology of phthalic acid and ester compounds, which is applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve problems such as analysis result errors, interference in the determination of migration components of special filters, and difficulty in component determination, so as to achieve convenient operation and eliminate Background interference of complex smoke components and the effect of avoiding background interference

Inactive Publication Date: 2018-10-19
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the very complex background generated when the cigarette is burned, it will seriously interfere with the determination of the migration components of the special filter. The determination of its components is very difficult, and the error of the analysis results is also very large.

Method used

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  • Detection device for migration quantity of phthalate ester compound and tributyl phosphate for special filter tip and detection method of detection device
  • Detection device for migration quantity of phthalate ester compound and tributyl phosphate for special filter tip and detection method of detection device
  • Detection device for migration quantity of phthalate ester compound and tributyl phosphate for special filter tip and detection method of detection device

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0056] Insert the temperature-measuring probe into the cigarette with the A-brand flavored compound filter at the starting point of the far lip end of the special filter, smoke it on an ordinary smoking machine, and use the temperature-measuring probe to measure the temperature passing through the far end of each puff. The temperature of the smoke at the starting point of lip filling, and the number of puffs of the whole cigarette is obtained;

[0057] According to the measured suction temperature and the number of suction ports, the detection device for the migration of phthalates and tributyl phosphate used in special filters is set, and the air temperature and temperature in each air heating chamber are set. The number of suction ports; the temperature settings are as follows: the first heating chamber 1' (the first port 36.5°C), the second heating chamber 2' (the second port 37.9°C), the third heating chamber 3' (the third port 41.2°C), the fourth heating chamber 4' (fourt...

Embodiment 2

[0064] Insert the temperature-measuring probe into the part where the bead is added to the far lip of the filter tip, and smoke it on an ordinary smoking machine, and use the temperature-measuring probe to measure the amount of smoke that passes through the bead during each puff. temperature, and obtain the puff number of the whole cigarette;

[0065] According to the measured suction temperature and the number of suction ports, the detection device for the migration of phthalates and tributyl phosphate used in special filters is set, and the air temperature and temperature in each air heating chamber are set. The number of suction ports; the temperature settings are as follows: the first heating chamber 1' (the first port 35.4°C), the second heating chamber 2' (the second port 36.5°C), the third heating chamber 3' (the third port 40.1°C), the fourth heating chamber 4' (fourth port 41.5°C), the fifth heating chamber 5' (fifth port 43.6°C), the sixth heating chamber 6' (sixth p...

Embodiment 3

[0072] Insert a temperature-measuring probe into the starting part of the particles on the far lip of the filter for a brand C cigarette containing particulate material, smoke it on an ordinary smoking machine, and use the temperature-measuring probe to measure the amount of particulate material that passes through each puff. The temperature of the smoke, and the number of puffs of the whole cigarette;

[0073] According to the measured suction temperature and the number of suction ports, the detection device for the migration of phthalates and tributyl phosphate used in special filters is set, and the air temperature and temperature in each air heating chamber are set. The number of suction ports; the temperature settings are as follows: the first heating chamber 1' (the first port 36.5°C), the second heating chamber 2' (the second port 37.9°C), the third heating chamber 3' (the third port 41.2 ℃), the fourth heating chamber 4' (fourth port 43.8 ℃), the fifth heating chamber ...

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Abstract

The invention relates to a detection device for migration quantities of a phthalate ester compound and tributyl phosphate for a special filter tip and a detection method of the detection device. The detection device comprises an air inlet, air heating cavities, a ten-way valve, a filter tip clamp, a flue gas capturer and a flue gas sucking machine, wherein the ten-way valve comprises a plurality of rotational air communicating holes, a fixed air communicating hole and a digital-control rotating disc; the number of the rotational air communicating holes is identical to that of the air heating cavities; each rotational air communicating hole is connected with one end of each air heating cavity; the other end of each air heating cavity is connected with the air inlet; the digital-control rotating disc is used for controlling whether the rotational air communicating holes are communicated with the fixed air communicating hole or not; the fixed air communicating hole, the filter tip clamp,the flue gas capturer and the flue gas sucking machine are connected in sequence. The detection device is simple in structure and convenient to operate, influence of complex flue gases can be reduced,and the detection method can be used as a novel analysis method for the migration quantities of the phthalate ester compound and the tributyl phosphate for the special filter tip.

Description

technical field [0001] The invention belongs to the technical field of physical and chemical testing of tobacco auxiliary materials, and in particular relates to a detection device for migration of phthalate compounds and tributyl phosphate used in special filters. At the same time, the invention also relates to a detection method using the detection device. Background technique [0002] With the international call for smoking ban and cigarette consumers' increasing concern for their own health, low-tar and low-hazard cigarettes will become the mainstream of cigarettes in the future, but the reduction of harm and coke will inevitably be accompanied by the loss of cigarette aroma and poor comfort. Cigarette flavoring and adding materials can set off and supplement the aroma of cigarettes, increase the concentration of smoke, improve taste, remove and cover up miscellaneous gases, reduce irritation, and can also give products a beautiful characteristic fragrance, highlighting ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/88
CPCG01N30/88G01N2030/884
Inventor 张承明王晋李晶刘欣孔维松杨叶昆陈建华耿永勤张涛李雪梅许永黄海涛杨光宇
Owner CHINA TOBACCO YUNNAN IND