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140results about How to "Good luminous stability" patented technology

Composite luminescent material and preparation method thereof and light emitting diode (LED) luminescent device

The invention relates to a composite luminescent material and a preparation method thereof and a light emitting diode (LED) luminescent device. The composite luminescent material comprises a plurality of layers of glass and fluorescent layers positioned among layers of the plurality of layers of glass, wherein a metal layer with a metal micro-nano structure is arranged in at least one of the layers of glass or on a contact surface of at least one of the layers of glass and the fluorescent layers. The metal micro-nano structure is introduced in the composite luminescent material and can form a surface plasma under the action of light rays emitted by a semiconductor chip and light rays emitted by fluorescent powder, and a strong exciting field is formed around the fluorescent powder by using local enhancement characteristic of the surface plasma, so the fluorescent powder can be fully excited and irradiated; moreover, by using energy transfer characteristic between the surface plasma and the fluorescent powder, radiation transition rate of the fluorescent powder is accelerated, and non-radiation transition of the fluorescent powder is suppressed, so the internal quantum efficiency of the fluorescent powder is improved, and the luminous efficiency of an LED packaged by the composite luminescent material is greatly enhanced.
Owner:OCEANS KING LIGHTING SCI&TECH CO LTD +1

Aluminosilicate blue fluorescent powder and preparation thereof

The invention relates to aluminosilicate blue phosphor powder and a preparation method thereof, and belongs to the technical field of luminescent material. The chemical formula of the aluminosilicate blue phosphor powder is Ba1-xAl2Si2O8:xEu<2+>, wherein x is more than 0 and less than 0.2. The preparation method comprises the following concrete steps: weighing barium salt, aluminum salt, silicic acid and europium oxide according to metering ratio of the elements in the chemical formula and proper amount of surfactant and fusing assistant; preparing a precipitating agent solution; dissolving the europium oxide by concentrated acid, and adding proper amount of deionized water to carry out water bath treatment; adding the barium salt, the aluminum salt and the surfactant, stirring the mixture, adding the precipitating agent solution into the mixture by multiple times, adjusting pH to more then or equal to 7, and continuously stirring the mixture for 0.5 to 4 hours; keeping standing or carrying out centrifugal precipitation, filtering, washing and drying the mixture to obtain a precursor; and after mixing the precursor and the fusing assistant evenly, placing the precursor and the fusing assistant into a muffle furnace protected by reducing atmosphere to calcine, so as to obtain the required phosphor powder. The preparation method adopts a one-time calcining technology and finishes doping at the same time of thermal decomposition of the precursor; and the prepared phosphor powder has the advantages of high luminous intensity and good stability and color rendering property, and is suitable to be used as near ultraviolet radiated blue phosphor powder of an LED excited by an InGaN tube core.
Owner:SICHUAN UNIV

Silicate green emitting phosphor powder for near ultraviolet excited light emitting diode (LED)

The invention relates to a synthesis method of silicate green emitting phosphor powder for a near ultraviolet excited light emitting diode (LED), which belongs to the preparation technology of rear earth phosphor powder. The chemical formula of the silicate is Ba1-xSiO3:xEu<2+>, wherein x is more than 0 and less than 0.1. The synthesis method of the silicate green emitting phosphor powder comprises following steps of measuring barium salt, silicic acid, europium nitrate and surface active agent and cosolvent with defined amount as required according to the chemical formula; adequately mixing the barium salt, the silicic acid, the europium nitrate, the surface active agent and ligand with defined amount, and then ball-milling, and adding a lubricant with defined amount in the ball milling process; filtering, washing and drying to obtain the precursor; and mixing the precursor with the cosolvent to be calcined under a reduction atmosphere to obtain the needed phosphor powder. The phosphor powder prepared by the method has the characteristics of wide laser excitation wavelength, high light emitting intensity, good crystallization and narrow distribution of granularity and is suitable for being used as the green emitting phosphor powder for the near ultraviolet excited white LED.
Owner:CHONGQING UNIV OF ARTS & SCI

<18>F-labeled aggregation-induced emission (AIE) fluorescent/positron emission tomography (PET) dual-mode probe, and preparation method and application thereof

The invention discloses an <18>F-labeled aggregation-induced emission (AIE) fluorescent / positron emission tomography (PET) dual-mode probe, and a preparation method and application thereof. The compound is denoted as <18>F-TPE-TEG, and has a following structure. The synthesis method of a labelled precursor of the compound comprises the following steps: firstly, adding 2-bromo-1,1,2-triphenylethylene, 4-hydroxyphenylboronic acid and tetrabutylammonium bromide into tetrahydrofuran, and taking K2CO3 and tetrakis(triphenylphosphine)palladium as catalysts to carry out a reaction to obtain 4-hydroxytetraphenylethylene; then dissolving triethylene glycol, triethylamine and p-toluenesulfonyl chloride in dichloromethane, and carrying out a reaction to obtain 8-p-toluenesulfonyloxy-3,6-dioxyoctanol;adding the 4-hydroxytetraphenylethylene, K2CO3, the 8-p-toluenesulfonyloxy-3,6-dioxyoctanol into acetonitrile, and carrying out a reaction to obtain 8-tetraphenylethyleneoxy-3,6-dioxyoctanol; and finally, dissolving the 8-tetraphenylethyleneoxy-3,6-dioxyoctanol, p-toluenesulfonyl chloride and triethylamine in dichloromethane, and carrying out a reaction to obtain the labelled precursor. The <18>F-labeled compound can be used as an AIE fluorescent / PET dual-mode probe to be applied to tumor imaging research.
Owner:ZHEJIANG UNIV

Method for preparing nitrogen-doped graphene quantum dot material

The invention provides a stable method for preparing a nitrogen-doped graphene quantum dot material. The preparation method comprises the following steps: dispersing networked reduced graphene oxide in concentrated nitric acid, and heating in an oil bath to a temperature of 140-160 DEG C while magnetic stirring, and reacting at a constant temperature for 12-48 hours under circulating water condensation; removing circulating condensate water, continuously evaporating at the constant temperature for 2-3 hours, and cooling to a room temperature; adding ultrapure water for ultrasonic dispersion, filtering, performing rotary evaporation and concentration on the filtrate, and filling in a dialysis bag of 3000-8000Da to dialyze for 24-48 hours; and performing rotary evaporation and concentrationon the dialysate again, and performing vacuum freeze drying, thereby obtaining the nitrogen-doped graphene quantum dots. The luminous stability of the nitrogen-doped graphene quantum dot is improved to a certain degree, and complicated passivating treatment and mixed element doping processes in the traditional process of preparing the doped quantum dots are effectively simplified. Moreover, the charge transfer capacity of the quantum dots is effectively improved, and the application potential in more fields such as photoelectricity, biomedicine and the like is facilitated.
Owner:NORTHWEST NORMAL UNIVERSITY

Method for preparing OLED light-emitting device with metal-enhanced fluorescence outer conversion layer

Provided is a method for preparing an OLED light-emitting device with a metal-enhanced fluorescence outer conversion layer. The invention provides a preparing method for a metal-enhanced fluorescence layer and an OLED device based on the method. The preparing method for the metal-enhanced fluorescence light-emitting layer includes the following steps of firstly, preparing a nanometer metal particle layer, wherein the nanometer metal particle layer is obtained by forming a metal film through vacuum evaporation and then conducting thermal treatment; secondly, preparing an organic fluorescence material solution, and evenly mixing the fluorescence material in high-molecular polymers; thirdly, preparing the metal-enhanced fluorescence outer conversion layer. The structure is prepared on the outer side of glass of an OLED, surface plasmas are formed on light waves emitted by the OLED device and metal nanometer particles on the outer side of the glass through the structure, and therefore the luminous intensity of fluorescent molecules is enhanced through the strong partial enhancing characteristic of the surface plasmas, the photoluminescence of the metal-enhanced fluorescence outer conversion layer of the OLED device is greatly enhanced. The OLED device with the metal-enhanced fluorescence outer conversion layer is simple in preparation process, low in device requirement and short in preparation cycle.
Owner:SHANGHAI UNIV

Quantum dots based luminescent solar concentrator based on spectral down-conversion technique, flat concentrating photovoltaic device and preparation method thereof

The invention discloses a quantum dots based luminescent solar concentrator (QDs-LSC) based on a spectral down-conversion technique, a flat concentrating photovoltaic device and a preparation method thereof. The QDs-LSC comprises a quantum dots based luminescent solar concentrating layer, and is characterized in that the upper surface of the quantum dots based luminescent solar concentrating layer is provided with a solar spectrum down-conversion layer; the lower surface of the quantum dots based luminescent solar concentrating layer and the upper surface of the solar spectrum up-conversion layer are provided with light-trapping layer glass pieces; the upper surface of the upper light-trapping layer glass piece is provided with a top antireflection layer for reducing the reflection of sunlight; and the lower surface of the lower light-trapping layer glass piece is provided with a bottom metal reflective layer. The flat concentrating photovoltaic device comprises solar panels arranged around the QDs-LSC. PCBs plated with conductive metal are fixedly disposed on the outer sides of the solar panels. The QDs-LSC can reduce the incident photon reflection loss and low-energy photon transmittance, thereby significantly improving the photon collection efficiency in the infrared band.
Owner:NINGBO UNIV

Synthetic method of silicate orange red fluorescent powder for white light light-emitting diode (LED)

A synthetic method of silicate orange red fluorescent powder for a white-light light-emitting diode (LED) belongs to a preparation technique of rare earth phosphor. The chemical formula of the rare earth phosphor is Sr3-x-yMySiO5:Xeu2+(M=Mg, Ca and Ba), wherein 0<x<0.1, and 0<y<0.2. The synthetic method particularly comprises steps of weighting corresponding alkali metal salt, ethyl orthosilicate and europium nitrate according to stoichiometric ratio of each element; then weighting a surface active agent and a fluxing agent which are 0.1-2wt% of a total mass of a drug; sufficiently hydrolyzing the ethyl orthosilicate, mixing the alkali metal salt, the europium nitrate, the surface active agent and the chelating agent in an aqueous solution, and enabling the molar ratio of the reactant and the chelating agent to be 1:2-6; and then mixing the two solutions, sufficiently stirring to form a transparent and clear solution, ageing under constant temperature, drying to obtain predecessor powder, evenly mixing the predecessor powder and a cosolvent, burning for 3-6 hours in a reducing atmosphere, enabling the burning temperature to be 1100 DEG C-1400 DEG C, and then obtaining the needed fluorescent powder. The fluorescent powder prepared by the synthetic method is wide in excitation wavelength, high in light intensity, good in crystallinity and narrow in size distribution and can be used for red fluorescent powder for the white-light LED.
Owner:重庆美地路艺建筑科技有限公司

Method for detecting treponema pallidum, quantum-dot labeled immunochromatography test paper and preparation method thereof

The invention relates to a medical immunodetection method and particularly relates to a method for using quantum-dot labeled immunochromatography test paper to detect treponema pallidum by an immunological method. The quantum-dot labeled immunochromatography test paper is characterized in that a plastic board is stuck with a glass cellulose membrane A, a glass cellulose membrane B of a quantum-dot labeled treponema pallidum IgG monoclonal antibody, a nitrocellulose membrane and water absorbing paper from bottom to top in sequence, wherein one end of the nitrocellulose membrane is provided with treponema pallidum polyclonal antibody and rabbit antimouse second antibody so as to form a detecting band T and a quality control band C; the quantum-dot labeled treponema pallidum IgG monoclonal antibody is positioned at one end of the glass cellulose membrane and corresponds to the detecting band T and the quality control band C, and the quantum-dot labeled treponema pallidum IgG monoclonal antibody is positioned at one end of a sampling point. The method has the advantages that high specificity of immunoreactions and the fluorescence characteristic of quantum dots are combined, so that the detection sensitivity is about 1000 times higher than that of the current commonly-used colloidal gold detection method.
Owner:北京华卫骥生物医药有限公司
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