High-low temperature urea grease composition with flame resistance and preparation method of high-low temperature urea grease composition

A urea-based lubricating grease, high and low temperature technology, applied in the field of lubricating grease, can solve the problems of inability to balance high and low temperature performance, fire, fire, etc., achieve good extreme pressure and anti-wear performance, simple preparation method, good flame resistance Effect

Inactive Publication Date: 2018-11-20
杭州新港润滑科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Taking steelmaking plants as an example, many mechanical equipment are operated under high-temperature environment conditions. Under the baking of high-temperature steel billets or molten steel, conventional grease is used as a combustible substance, which is likely to catch fire or even cause a fire, resulting in major economic losses. loss
[0003] Aiming at the current situation that conventional lubricating grease cannot balance high and low temperature performance, and does not have anti-flammability effect, we have designed a new urea-based grease formula, and on this basis, developed high-low temperature urea-based grease with anti-flammability function, While ensuring that the equipment can have a good lubricating effect in a wide temperature range, it can reduce fire hazards and has a good application prospect

Method used

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  • High-low temperature urea grease composition with flame resistance and preparation method of high-low temperature urea grease composition
  • High-low temperature urea grease composition with flame resistance and preparation method of high-low temperature urea grease composition

Examples

Experimental program
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Effect test

Embodiment 1

[0022] A flame-resistant high and low temperature urea-based grease composition, the composition of which is as follows:

[0023] Synthetic Base Oil: Pentaerythritol Ester, 83.0g

[0024] Polyurea thickener: diphenylmethane diisocyanate MDI (3.5g), octadecylamine (4.5g), aniline (1.0g)

[0025] Polyvinyl alcohol: 2.0g

[0026] Polyisobutylene glue: 2.0g

[0027] Zinc dialkyldithiophosphate: 2.0g

[0028] Micro-nano borate T361A: 2.0g

[0029] production method:

[0030] (1) Put 50% of the total weight of base oil into the first reaction kettle, heat to 50-60°C, then add all octadecylamine and aniline, stir and heat to 70-80°C.

[0031] (2) Put the remaining base oil into the second reaction kettle, raise the temperature to 50-60°C, then add MDI, stir and raise the temperature to 70-80°C.

[0032] (3) Add all the amine solution in the first reaction kettle to the second reaction kettle under the condition of non-stop stirring.

[0033] (4) Keep the temperature at 100-110...

Embodiment 2

[0040] A flame-resistant high and low temperature urea-based grease composition, the composition of which is as follows:

[0041] Synthetic base oil: trimethylolpropane ester (40.0g), pentaerythritol ester (38.0g)

[0042] Polyurea thickener: toluene diisocyanate TDI (4.0g), ethylenediamine (0.7g), octadecylamine (6.3g)

[0043] Polyvinyl alcohol: 3.0g

[0044] Polyisobutylene glue: 3.0g

[0045] Zinc dialkyldithiophosphate: 3.0g

[0046] Micro-nano borate T361A: 2.0g

[0047] production method:

[0048] (1) Put 50% of the total weight of base oil into the first reaction kettle, heat to 50-60°C, then add all octadecylamine and ethylenediamine, stir and heat to 70-80°C.

[0049] (2) Put the remaining base oil into the second reaction kettle, raise the temperature to 50-60°C, then add MDI, stir and raise the temperature to 70-80°C.

[0050] (3) Add all the amine solution in the first reaction kettle to the second reaction kettle under the condition of non-stop stirring.

...

Embodiment 3

[0058] A flame-resistant high and low temperature urea-based grease composition, the composition of which is as follows:

[0059] Synthetic Base Oil: Trimethylolpropane Ester, 79.0g

[0060] Polyurea thickener: diphenylmethane diisocyanate MDI (5.0g), aniline (1.4g), n-octylamine (3.2g)

[0061] Polyvinyl alcohol: 3.0g

[0062] Polyisobutylene glue: 3.4g

[0063] Zinc dialkyldithiophosphate: 3.0g

[0064] Micro-nano borate T361A: 2.0g

[0065] production method:

[0066] (1) Put 50% of the total weight of base oil into the first reaction kettle, heat to 50-60°C, then add all n-octylamine and aniline, stir and heat to 70-80°C.

[0067] (2) Put the remaining base oil into the second reaction kettle, raise the temperature to 50-60°C, then add MDI, stir and raise the temperature to 70-80°C.

[0068] (3) Add all the amine solution in the first reaction kettle to the second reaction kettle under the condition of non-stop stirring.

[0069] (4) Keep the temperature at 100-110°...

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Abstract

The invention discloses high-low temperature urea grease composition with flame resistance and a preparation method of the high-low temperature urea grease composition. The high-low temperature urea grease composition is prepared from the following components in parts by weight: 67-87 parts of synthetic base oil, 5-15 parts of a polyurea-based thickener, 1-5 parts of polyvinyl alcohol, 3-5 parts of polyisobutylene gel, 2-3 parts of zinc dialkyl dithiophosphate and 2-5 parts of micro-nano borate T36A. The preparation method of the composition comprises the following steps: feeding the syntheticbase oil and the polyurea-based thickening agent into an oil-bath heating reaction kettle, stirring the mixture uniformly, and performing saponification to form grease to prepare basic grease; then adding polyvinyl alcohol, the polyisobutylene gel, zinc dialkyldithiophosphate and micro-nano borate T361A sequentially to the reaction kettle, and stirring and dispersing the mixture uniformly; finally, performing homogenization by a homogenizer or grinding by a three-roller machine to prepare the high-low temperature urea-based lubricating grease with a flame resistant function.

Description

technical field [0001] The invention belongs to the field of lubricating grease, in particular to a flame-resistant high-low temperature urea-based lubricating grease composition and a preparation method thereof. Background technique [0002] Grease is a lubricant in solid or semi-solid state, generally composed of base oil, thickener and additives, etc. It can adhere well to the surface of friction parts of mechanical equipment, thereby reducing friction and wear. When the operating conditions of mechanical equipment are relatively complicated, especially when the ambient temperature changes greatly, it requires that the grease can maintain a good lubricating effect in a wide temperature range, that is to say, it must have good high and low temperature performance. Taking steelmaking plants as an example, many mechanical equipment are operated under high-temperature environment conditions. Under the baking of high-temperature steel billets or molten steel, conventional grea...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M169/04C10N50/10C10N30/06C10N30/08
CPCC10M169/044C10M2201/087C10M2205/02C10M2207/2835C10M2209/04C10M2215/04C10M2215/062C10M2215/14C10M2223/045C10N2010/04C10N2020/06C10N2030/06C10N2030/08C10N2050/10
Inventor 刘仁德
Owner 杭州新港润滑科技有限公司
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