Recycling device for solvents with high viscosity in dangerous waste treatment field, skid-mounted structure and method thereof
A solvent recovery device, high viscosity technology, applied in separation methods, chemical instruments and methods, distillation separation, etc., can solve the problems of high solvent surface tension, equipment installation and dispersion, separation and recovery difficulties, etc., to reduce residence time and equipment discharge. The effect of tight cloth, flexible and convenient movement
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Embodiment 1
[0068] The liquid hazardous waste to be treated mainly contains 30% propylene glycol methyl ether acetate, 30% light phase, 30% water and 10% impurities.
[0069] In the first step, the liquid to be treated is transported to the rectification kettle, heated and vaporized, and then enters the rectification tower for separation;
[0070] The second step is to adjust the rectification operating conditions and carry out partial reflux rectification operation. The temperature of the top of the rectification tower is 60°C, the temperature of the bottom of the tower is 130°C, and the number of theoretical plates is 20. The gas produced at the top of the tower is collected by the condenser and Contains light phase and water after being condensed, and the light phase and water are stored in the waste liquid storage device, and the heavy phase is extracted from the rectification column, which contains solvent and impurities, and the heavy phase is sent to the evaporator for evaporation a...
Embodiment 2
[0073] The liquid hazardous waste to be treated mainly contains 30% triethylene glycol, 30% light phase, 30% water and 10% impurities.
[0074] In the first step, the liquid to be treated is transported to the rectification kettle, heated and vaporized, and then enters the rectification tower for separation;
[0075] The second step is to adjust the rectification operating conditions and carry out partial reflux rectification operation. The temperature at the top of the rectification tower is 110°C, the temperature at the bottom of the tower is 220°C, and the number of theoretical plates is 20. The gas produced at the top of the tower is collected by the condenser and The light phase and water are stored in the waste liquid storage device after being condensed, and the heavy phase is extracted from the rectification column, which contains the solvent triethylene glycol and impurities, and the heavy phase is sent to the evaporator for evaporation and separation. The concentrati...
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