A kind of preparation method of anti-marine organism adhesion cage coating
A technology for marine organisms and coatings, applied in the field of coatings, can solve problems such as toxicity and harm of cage coatings, environmental hazards, etc., and achieve the effects of ensuring effectiveness, reducing surface tension, and improving mechanical properties
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Embodiment 1
[0041] A preparation method of an anti-adhesion net cage coating for marine organisms, said preparation method comprising the following steps:
[0042] S.1 Preparation of modified nano-silica: condense the mixed solution of nano-silica and silane coupling agent in the solution to obtain modified nano-silica. The preparation process is as follows:
[0043] (a1) Surface activation: according to parts by weight, put 100 parts of fumed nano-silica and 2 parts of glacial acetic acid in the reaction kettle, then pass water vapor into it, raise the temperature to 115 ° C, and keep the reaction kettle The air pressure is 8.0MPa, after activating for 120 minutes, it is lowered to room temperature, and after vacuum drying and grinding, the surface-activated nano-silica is obtained;
[0044] (a2) Modification: In parts by weight, take 20 parts of surface-activated nano-silica and disperse it into 100 parts of ethanol, and add γ-methacryloyloxypropyl trimethyl to it while stirring Oxysilan...
Embodiment 2
[0053] A preparation method of an anti-adhesion net cage coating for marine organisms, said preparation method comprising the following steps:
[0054] S.1 Preparation of modified nano-silica: condense the mixed solution of nano-silica and silane coupling agent in the solution to obtain modified nano-silica, wherein the preparation process is as follows:
[0055] (a1) Surface activation: according to parts by weight, put 100 parts of fumed nano-silica and 5 parts of glacial acetic acid in the reaction kettle, then pass water vapor into it, raise the temperature to 110 ° C, and keep the reaction kettle The air pressure is 10.5MPa, after activation for 120 minutes, it is lowered to room temperature, and after vacuum drying and grinding, the surface-activated nano-silica is obtained;
[0056] (a2) Modification: In parts by weight, take 35 parts of surface-activated nano-silica and disperse it into 100 parts of ethanol, and add γ-methacryloyloxypropyl trimethyl to it while stirrin...
Embodiment 3
[0065] A preparation method of an anti-adhesion net cage coating for marine organisms, said preparation method comprising the following steps:
[0066] S.1 Preparation of modified nano-silica: condense the mixed solution of nano-silica and silane coupling agent in the solution to obtain modified nano-silica, wherein the preparation process is as follows:
[0067] (a1) Surface activation: according to parts by weight, put 100 parts of fumed nano-silica and 3 parts of glacial acetic acid in the reaction kettle, then pass water vapor into it, raise the temperature to 115 ° C, and keep the reaction kettle The air pressure is 9MPa, after activation for 60 minutes, it is lowered to room temperature, and after vacuum drying and grinding, the surface-activated nano-silica is obtained;
[0068] (a2) Modification: In parts by weight, take 30 parts of surface-activated nano-silica and disperse it into 100 parts of ethanol, and add γ-methacryloyloxypropyl trimethyl to it while stirring O...
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