Modified polymers and stable emulsions comprising same
A technology of polymers and polymer chains, which can be used in transportation and packaging, plant fibers, textiles and papermaking, and can solve expensive and environmentally unfriendly problems
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[0057] Embodiments of the present invention are further illustrated with reference to the following non-limiting examples.
[0058] Synthesis of Aqueous Polymer Emulsion Terminated by Blocked Isocyanate
[0059] Polyols in the form of hydroxylated polybutadiene (Poly R-45HTLO) was combined with dimethylolpropionic acid (DMPA), triethylamine (NeT3) and isophorone diisocyanate (IPDI) in the following amounts:
[0060] Table 1
[0061]
[0062]
[0063] These materials were combined in a solvent (methyl ethyl ketone) at room temperature to form a dispersion such that the final solids content of the dispersion was 40%. The temperature of the dispersion was raised to 80°C and the dispersion was stirred for 2 hours. The temperature was maintained while an excess of cyclohexanone oxime (19.3 g) was added to ensure that most, if not all, of the terminal isocyanate groups were blocked. After adding the oxime, the emulsion is prepared by adding water to the solvent phase or...
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