A class of iridium coordination compounds as phosphorescence materials, preparation method and applications thereof
A technology of iridium complexes and phosphorescent materials, applied in the directions of luminescent materials, compounds containing elements of Group 8/9/10/18 of the periodic table, chemical instruments and methods, etc., can solve the problems of increasing the complexity of material production and achieve Simple operation and high luminous efficiency
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Embodiment 1
[0034] The synthesis of iridium complex 1, the reaction equation is as follows:
[0035] (1) Preparation of the main ligand
[0036]
[0037] (2) Synthesis of chlorine-bridged dimers
[0038]
[0039] (3) Target synthesis
[0040]
Embodiment 2
[0042] The synthesis of iridium complex 2, the reaction equation is as follows:
[0043] (1) Preparation of the main ligand
[0044]
[0045] (2) Synthesis of chlorine-bridged dimers
[0046]
[0047] (3) Target synthesis
[0048]
Embodiment 3
[0050] The synthesis of iridium complex 12, reaction equation is as follows:
[0051] (1) Preparation of the main ligand
[0052]
[0053] (2) Synthesis of chlorine-bridged dimers
[0054]
[0055] (3) Target synthesis
[0056]
[0057] like figure 1 As shown, the structure of an organic electroluminescent device (OLED) includes a glass substrate 1, an anode layer 2, a hole injection layer 3, a hole transport layer 4, a light emitting layer 5, an electron transport layer 6, and an electron injection layer sequentially stacked and combined. layer 7 and cathode layer 8. The iridium phosphorescent material prepared by the present invention is applied in the light-emitting layer of the OLED, and Table 1 shows the composition of each layer of the OLED in application examples 1-3.
[0058] Table 1
[0059]
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