Screening and identifying method for TLR vaccine adjuvants
A technology of vaccine adjuvant and identification method, which can be used in material inspection products, measuring devices, instruments, etc., and can solve problems such as unclearness
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[0088] Experiment A: Lysis and pre-separation of virus, the operation steps are as follows:
[0089] VV-WR strain (VR-1354) was purchased from ATCC. Add 10 ml of PBS containing 1% Triton X-100 to dissolve 1 mg of VV virus pellet, and incubate at 37°C for 1 hour to extract the total protein.
[0090] In order to remove the effect of detergent, the total protein needs to go through the following dialysis step: add the lysate mixed with the total viral protein into the Slide-A-Lyzer dialysis card (2 kDa MWCO) (Thermo Scientific, Cat. No. 87719), and dialyze at 4°C overnight. The specific dialysis method is: dialyze in 1xPBS buffer solution at 4°C, and change the dialysate every 3 hours for a total of 3 times.
[0091] The mixture was centrifuged at 15,000 g for 30 min to remove insoluble precipitates.
[0092] The protein concentration of the mixture was determined by BCA method (Sanko, Cat. No. C503021-0500).
[0093] 250 μg of the mixture was ultrafiltered through 30 kD MWC...
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