Preparation method for carbon-containing quantum dot white light emitting room temperature ionic liquid
A room temperature ionic liquid, carbon quantum dot technology, applied in chemical instruments and methods, nano-carbon, luminescent materials, etc., can solve the problems of low luminous efficiency, complicated construction methods, etc., achieve simple operation, simple and feasible preparation method, and broaden the spectrum. range effect
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Embodiment 1
[0052] Preparation of Green Light Emitting Carbon Quantum Dots
[0053] Weigh 0.16g o-phenylenediamine, 0.083g 1-aminopropyl-3-methylimidazolium bromide, stir and dissolve in 10mL deionized water; React for 12 hours; after the reaction, turn off the oven, cool to room temperature naturally, and obtain a reaction solution, measure the fluorescence quantum yield of carbon quantum dots in the reaction solution obtained to be 6.94%; further use the reaction solution through silica gel column chromatography, and use ethyl acetate The ester was used as the eluent for purification, and the solvent was evaporated to dryness to obtain green light-emitting carbon quantum dots.
Embodiment 2
[0055] Preparation of Green Light Emitting Carbon Quantum Dots
[0056] As described in Example 1, the difference is that the amount of 1-aminopropyl-3-methylimidazolium bromide added is 0 g, and the fluorescence quantum yield of carbon quantum dots in the resulting reaction solution is 7.90%.
Embodiment 3
[0058] Preparation of Green Light Emitting Carbon Quantum Dots
[0059] As described in Example 1, the difference is that the addition of 1-aminopropyl-3-methylimidazolium bromide is 0.17g, and the fluorescence quantum yield of carbon quantum dots in the resulting reaction solution is 10.31%. After purification, the obtained The fluorescence quantum yield of green light-emitting carbon quantum dots is 11.68%.
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