Production method for rumen-bypassing preparation, and granules obtained by means of production method for rumen-bypassing preparation
A rumen-passing and preparation technology, which is used in food ingredients as coating agents, animal feed molding or processing, food science, etc., can solve difficult problems and achieve high stability
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Embodiment 1
[0070] Example 1: Rumen Passed Vitamin D 3 Preparation of formulations and analysis of the resulting formulations
Embodiment 1-1
[0071] Example 1-1: Rumen Passed Vitamin D 3 Preparation of formulations and determination of their particle size distribution
[0072] In this example, a vitamin D3 formulation was prepared and its particle size distribution is shown.
[0073] 100 kg of hydrogenated palm oil was melted at 72°C. To this melt was added 6.25 g of vitamin D dissolved in soybean oil 3 , stir until uniform. The obtained solution was sent to a vibrating granulator having a die hole diameter of 0.7 mm, vibration of 1000 to 10000 Hz was applied, and sprayed into cold air. Rumen-passed vitamin D against coagulation 3 , the particle size distribution was measured based on the particle size measurement method (sieving method) of the Japanese Pharmacopoeia. The vibration is set as a sine wave with a p-p value of 5 mm.
[0074] In the above, the vibration granulation device 100 used in this embodiment is as figure 1 shown. like figure 1 As shown, the vibration granulation apparatus 100 used in t...
Embodiment 1-2
[0081] Example 1-2: Analysis of the structure of the obtained particles
[0082] According to the sieving method of the Japanese Pharmacopoeia, particles having a particle diameter of 1000 μm to 1519 μm were obtained from the obtained particles, and analyzed in more detail. In this example, especially the distribution of pore size was analyzed.
[0083] The pore size was measured by mercury intrusion porosimetry using a mercury porosimeter. The measurement was performed using Auto Pore III (manufactured by Micrometrics). The particles having a particle size of 1000 μm to 1519 μm obtained above were degassed, mercury was injected into the particles, and the relationship between the amount of mercury infiltrated into the particles and the pressure applied at that time was investigated. The pore size was calculated using the Washburn equation,
[0084] D=-4γCOSθ / P
[0085] {where, D is the pore diameter, γ is the surface tension of mercury (ie 480 dynes / cm), and θ is the cont...
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