A large-size low-loss optical fiber preform and its manufacturing method
A technology of optical fiber preform and manufacturing method, which is applied in the field of large-size and low-loss optical fiber preform and its manufacturing, and can solve the problems of inability to manufacture optical fiber preform and inability to manufacture large-size and low-loss optical fiber preform, etc.
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Embodiment 1
[0048] The powder mandrel is prepared by the axial vapor deposition method (VAD method), and then the prepared powder mandrel is dehydroxylated, fluorine doped and vitrified in a graphite sintering furnace, and Cl is introduced into the sintering furnace during dehydration. 2 gas and He gas, Cl 2 The gas flow rate is 1000mL / min, the He gas flow rate is 20L / min, and the dehydration temperature is 1050°C. During dehydration, the powder mandrel moves from top to bottom at a moving speed of 8mm / min; after dehydration, the powder mandrel rises to the upper part of the sintering furnace , into SiF 4 gas and He gas, SiF 4 The flow ratio of gas and He gas is 4:1, in which the flow rate of He gas is 30L / min, the temperature of sintering furnace is 1400℃ when doped with fluorine, and the powder mandrel moves from top to bottom at a speed of 10mm / min; finally the powder mandrel Move from top to bottom for vitrification treatment, the moving speed is 4mm / min, only He gas is fed into the...
Embodiment 2
[0056] The powder mandrel is prepared by the axial vapor deposition method (VAD method), and then the prepared powder mandrel is dehydroxylated, fluorine doped and vitrified in a graphite sintering furnace, and Cl is introduced into the sintering furnace during dehydration. 2 gas and He gas, Cl 2 The gas flow rate is 900mL / min, the He gas flow rate is 25L / min, and the dehydration temperature is 900°C. During dehydration, the powder mandrel moves from top to bottom at a moving speed of 7mm / min; after dehydroxylation, the powder mandrel rises to the upper part of the sintering furnace , into CF 4 gas and He gas, CF 4 The flow ratio of gas and He gas is 3:1, the flow rate of He gas is 40L / min, the temperature of the sintering furnace is 1100℃ when doped with fluorine, and the powder mandrel moves from top to bottom at a speed of 8mm / min; finally the powder mandrel Move from top to bottom for vitrification treatment, the moving speed is 3mm / min, only He gas is passed into the si...
Embodiment 3
[0064] The powder mandrel is prepared by the axial vapor deposition method (VAD method), and then the prepared powder mandrel is dehydroxylated, fluorine doped and vitrified in a graphite sintering furnace, and Cl is introduced into the sintering furnace during dehydration. 2 gas and He gas, Cl 2 The gas flow rate is 1100mL / min, the He gas flow rate is 15L / min, the dehydration temperature is 1100°C, the powder mandrel moves from top to bottom during dehydration, and the moving speed is 10mm / min; after the dehydration is completed, the powder mandrel rises to the upper part of the sintering furnace , into SF 6 Gas and He gas, SF 6The flow ratio of gas and He gas is 5:1, the flow rate of He gas is 20L / min, the temperature of sintering furnace is 1500℃ when doped with fluorine, and the powder mandrel moves from top to bottom at a speed of 9mm / min; finally the powder mandrel Move from top to bottom for vitrification treatment, the moving speed is 6mm / min, only He gas is fed into...
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