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Hydrofining catalyst performance prediction method

A technology for hydrorefining and performance prediction, applied in chemical property prediction, neural learning method, chemical statistics and other directions, can solve problems such as affecting the economic benefits of enterprises, waste of manpower and material resources, long operation cycle, etc., to save research and development costs, predicting The effect of high precision and strong generalization ability

Pending Publication Date: 2019-04-19
CNOOC OIL & PETROCHEMICALS CO LTD +2
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  • Abstract
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Problems solved by technology

[0003] At present, the research method of catalyst research and development through traditional experimental means not only has a certain degree of blindness, but also requires a large number of experiments to try and screen, which wastes manpower and material resources, and because the process is mostly a continuous device, it usually requires a long operation period for research. It is difficult to respond to the rapidly changing market and provide timely feedback to provide solutions, which affects the economic benefits of the enterprise

Method used

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  • Hydrofining catalyst performance prediction method

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Embodiment 1

[0033] Hydrotreating catalyst performance prediction method, the process is as follows figure 1 shown, including the following steps:

[0034] 1) Hydrofining catalyst preparation

[0035] Fully mix 100g of pseudo-boehmite powder, 3ml of nitric acid, 3g of safflower powder, and 100ml of pure water, and knead them into shape through a twin-screw extruder. After calcination at a high temperature of ℃, the hydrorefining catalyst carrier is prepared. The basic nickel carbonate solid is prepared into a saturated solution, the content in terms of oxides is 20.0wt%, the hydrogenation refining catalyst carrier and the basic nickel carbonate solution are fully mixed, and the hydrogenated Refined catalyst;

[0036] 2) Performance evaluation of hydrofining catalyst

[0037] Install the hydrorefining catalyst in the hydrogenation microreactor, select the reaction pressure to be 1.6MPa, the reaction temperature to be 240°C, the hydrogen-to-oil ratio to be 100, and the volume space veloc...

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Abstract

The invention discloses a hydrofining catalyst performance prediction method which comprises the following steps: obtaining basic data during crude oil hydrogenation reaction, and normalizing the datato form a database; Establishing a generalized regression neural network model, taking the data influencing the properties of the hydrofining catalyst in the obtained database as input data, and taking the data related to the properties of the product obtained after the hydrogenation reaction as output data; Training the generalized regression neural network model; And predicting the performanceof the hydrofining catalyst. According to the method, the performance of the catalyst can be quickly and effectively predicted, unnecessary repeated labor and energy consumption are reduced, the modelis high in learning speed, high in generalization ability and high in prediction precision, and the performance of the hydrofining catalyst during crude oil hydrogenation catalytic reaction can be quickly and accurately predicted.

Description

technical field [0001] The invention relates to the field of catalyst performance prediction. More specifically, it relates to a method for predicting the performance of a hydrorefining catalyst. Background technique [0002] At present, with the gradual decline in the quality of crude oil, people's demand for pure oil products continues to increase. In the process of petroleum refining, more and more attention is paid to hydrogenation technology, and the most important part of hydrogenation technology is the catalyst. use. [0003] At present, the research method of catalyst research and development through traditional experimental means not only has a certain degree of blindness, but also requires a large number of experiments to try and screen, which wastes manpower and material resources, and because the process is mostly continuous equipment, it usually requires a long operation period for research. It is difficult to respond to the rapidly changing market and provide...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G16C20/30G16C20/10G16C20/70G16C20/90G06N3/04G06N3/08C10G45/04
CPCG06N3/08C10G45/04C10G2300/70G06N3/045
Inventor 李昊于群杨国明马致远辛靖张博陈松侯章贵高杨吴颖
Owner CNOOC OIL & PETROCHEMICALS CO LTD
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