Non-evapotranspiration type thin film getter and preparation method thereof
A non-evaporative, getter technology, applied in separation methods, chemical instruments and methods, dispersed particle separation, etc., can solve the problems of limiting the service life of components, maintaining the vacuum degree of the cavity, etc., to extend the service life, increase the Inhalation capacity, the effect of increasing the specific surface area
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Embodiment 1
[0039] Ti films were deposited on silicon wafers with inclination angles of 50° and 70° respectively, and columnar films with inclination angles of 29° and 46° were deposited. The inclination angle conforms to the theoretical formula tanα=2×tanβ, and the theoretical values of the β angles should be 31° and 54° respectively. After testing, the porosity of the film is 25% and 55%, respectively, which indicates that the oblique-angle deposition method of this embodiment can deposit a porous film.
[0040] Then, a gold layer is covered on the surface of the film to obtain a film structure such as image 3 shown. Among them, 300 is a columnar porous thin film getter, and 301 is a 10-50 thick nanometer protective layer covered on the surface of the thin film getter. The structure is dense. The protective layer can prevent the surface of the getter from being polluted when it is not activated.
[0041] Under the activation conditions of 300°C and 1h, the above-mentioned film gett...
Embodiment 2
[0043] Before depositing the film, the cavity is wet-etched to etch out such as figure 2 The cavity is inclined at an angle of 54.7°. Next, a thin film is deposited in the cavity to obtain a porous columnar thin film. After testing, its air-absorbing capacity is about 20 times that of the non-columnar film.
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