Low-loss ferrite material and preparation method thereof
A ferrite material, low-loss technology, applied in the direction of inorganic material magnetism, chemical instruments and methods, iron compounds, etc., can solve the problems of limitations, large losses, etc., to improve reaction speed, reduce hysteresis loss, and reduce reaction the effect of time
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Embodiment 1
[0020] A kind of low-loss ferrite material, its raw material comprises main component and auxiliary component, and described main component comprises Fe 2 o 3 , Mn 2 o 3 , ZnO; the auxiliary components include CaO, La 2 (CO 3 ) 3 ·8H 2O, CeO 2 ·nH 2 O.
[0021] The preparation method of the low-loss ferrite material, the method comprises the following steps: Fe 2 o 3 , Mn 2 o 3 , ZnO and La 2 (CO 3 ) 3 ·8H 2 O, CeO 2 ·nH 2 O is mixed in an agate mortar, firstly ground, dried, added with CaO, secondly ground to fine powder, heat treated, mixed with lubricant and binder, three times grounded, and spray granulated to obtain a low-loss ferrite material.
Embodiment 2
[0023] A kind of low-loss ferrite material, its raw material comprises main component and auxiliary component, and described main component comprises Fe 2 o 3 , Mn 2 o 3 , ZnO; the auxiliary components include CaO, La 2 (CO 3 ) 3 ·8H 2 O, CeO 2 ·nH 2 O;
[0024] Wherein, the main component includes 53.2mol% Fe 2 o 3 , 35.8mol% Mn 2 o 3 , 11.0mol% ZnO; relative to the main component, the auxiliary components include 300ppm CaO, 200ppm La 2 (CO 3 ) 3 ·8H 2 O, 260ppm CeO 2 ·nH 2 O.
[0025] The preparation method of the low-loss ferrite material, the method comprises the following steps: Fe 2 o 3 , Mn 2 o 3 , ZnO and La 2 (CO 3 ) 3 ·8H 2 O, CeO 2 ·nH 2 O is mixed in an agate mortar, first ground, dried, added with CaO, secondly ground to fine powder, placed in a box-type resistance furnace for heat treatment, mixed with lubricant and binder, three times ground, and spray granulated to obtain Low loss ferrite material.
Embodiment 3
[0027] A kind of low-loss ferrite material, its raw material comprises main component and auxiliary component, and described main component comprises Fe 2 o 3 , Mn 2 o 3 , ZnO; the auxiliary components include CaO, La 2 (CO 3 ) 3 ·8H 2 O, CeO 2 ·nH 2 O;
[0028] Wherein, the main component includes 53.5mol% Fe 2 o 3 , 35.0mol% Mn 2 o 3 , 11.5mol% ZnO; relative to the main component, the auxiliary components include 10ppm CaO, 300ppm La 2 (CO 3 ) 3 ·8H 2 O, 100ppm CeO 2 ·nH 2 O;
[0029] The La 2 (CO 3 ) 3 ·8H 2 The preparation method of O is as follows: Add sodium bicarbonate solution to the lanthanum chloride solution at a rate of 0.07mL / s, then filter with suction, wash the obtained solid, and dry to obtain La 2 (CO 3 ) 3 ·8H 2 O;
[0030] The volume ratio of the lanthanum chloride solution and the sodium bicarbonate solution is 1:6.5; the concentration of the lanthanum chloride solution is 2mol / L; the concentration of the sodium bicarbonate soluti...
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