A kind of blue phase liquid crystal film and its preparation method and use
A technology for blue phase liquid crystal and its application, which is applied in the field of blue phase liquid crystal film and its preparation. It can solve the problems of narrow blue phase temperature range, low Q value, and high threshold value, and achieve the purpose of reducing the unevenness of lattice size distribution and wavelength stability. Improve the effect of good application prospects
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no. 1 approach
[0035] The first embodiment of the present invention provides a blue phase liquid crystal film, the components of which include: 30wt% liquid crystal monomer C6M participating in polymerization, 59.5wt% liquid crystal molecule HTG135200-100 not participating in polymerization, 2.9-3.7wt % chiral dopant, 5wt% cross-linking agent, 0.2-2wt% photoinitiator and 0.5-2wt% small molecule dye.
[0036] Preferably, the thickness of the blue phase liquid crystal film is 10-500 μm. When the thickness of the blue-phase liquid crystal film is less than 10 μm, the period number of the periodic structure in the blue-phase liquid crystal film will be less, which is not enough to provide high enough reflectivity and band edge density, and is not enough to make the high threshold band edge reach Threshold to emit dual-wavelength laser; when the thickness of the blue-phase liquid crystal film is higher than 500 μm, the temperature of the upper surface and the lower surface is difficult to be unif...
no. 2 approach
[0045] figure 1 It is a flowchart of a preparation method of a blue phase liquid crystal film provided in the second embodiment of the present invention.
[0046] Such as figure 1 As shown, the method includes step S101 to step S104.
[0047] In step S101, 30wt% of polymerizable liquid crystal monomer C6M, 59.5wt% of liquid crystal molecules HTG135200-100 that do not participate in polymerization, 2.9-3.7wt% of chiral dopant, 5wt% of cross-linking agent, 0.2- 2wt% photoinitiator and 0.5-2wt% small molecule dye are put into a container and mixed uniformly to obtain a mixture.
[0048] Step S102, after heating the mixture to the liquid crystal clearing point, pouring it into a liquid crystal cell with a thickness of 10-500 μm.
[0049] Wherein, the liquid crystal clearing point temperature of most liquid crystals in the present invention is generally above 80°C.
[0050] In step S103, the temperature of the liquid crystal cell is lowered to make the mixture reach a blue phas...
Embodiment 1
[0062] After mixing 59.5wt% of liquid crystal molecule HTG135200-100 and 30wt% of polymerizable liquid crystal monomer C6M, 0.5wt% of photoinitiator I-651, 5wt% of TMPTA, 3.3wt% of R5011 and 0.5 Wt% small molecular dyes are put into a container and mixed evenly to obtain a liquid crystal mixture. Among them, coumarin 6 is selected as the small molecular dye.
[0063] The above-mentioned liquid crystal mixture is heated to its liquid crystal clearing point or above its liquid crystal clearing point, heated to 90° C. in Example 1, and poured into a liquid crystal cell with a thickness of 50 μm between the liquid crystal cells.
[0064] Cool the liquid crystal cell to the blue phase liquid crystal state (BPI state), and control the cooling speed at 0.5°C / min
[0065] Irradiate with ultraviolet light with a wavelength of 385nm for 80s.
[0066] The liquid crystal cell is disassembled, and the blue-phase liquid crystal polymer film is taken out to obtain a blue-phase liquid cryst...
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