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A method for measuring the thickness of steel wire coating

A coating thickness and measurement method technology, which is applied in the field of material microstructure inspection, can solve problems such as low reliability of coating thickness values, unsatisfactory test results, and unrealistic problems, so as to achieve intuitive measurement results, accurate and reliable calculation results, and easy operation. simple effect

Active Publication Date: 2020-11-24
INST OF RES OF IRON & STEEL JIANGSU PROVINCE +2
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The non-destructive testing method has certain special requirements on the materials of the substrate and the coating, and the test results have a large error compared with the destructive testing; the metallographic method needs to ensure that the prepared cross-sectional sample is perpendicular to the coating to be tested. It is relatively easy to implement for block samples, but it is basically impossible for steel wires with a diameter of less than 1mm, especially 0.06mm; the Coulomb method is only suitable for flat samples, and it is impossible to measure the thickness of steel wire coatings
At present, there is also a scanning electron microscope to measure the coating thickness of the steel wire section, but for very thin steel wire, it cannot be guaranteed that the prepared cross-sectional sample is a vertical plane in the direction of the steel wire length, and a slight inclination will cause a large measurement error, so it is measured. Confidence is too low for coating thickness values
The existing coating thickness testing methods can solve the measurement of the thickness of large samples, but for such thin steel wires, there are shortcomings such as inability to measure or samples cannot be prepared, resulting in unsatisfactory test results.

Method used

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  • A method for measuring the thickness of steel wire coating

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Embodiment 1

[0021] A method for measuring the thickness of steel wire coating, including the following steps:

[0022] (1) Measurement: Measure and calculate the diameter D of the cut steel wire containing the coating by using a vernier caliper or a micrometer to take the average of multiple measurements 0 ;

[0023] Table 1 Diameter D of cutting steel wire with coating 0 Measurement and calculation results

[0024] Number of measurements12345 average value D0

0.43mm 0.42mm 0.44mm 0.43mm 0.43mm 0.43mm

[0025] (2) Sample preparation: mount and sample the cut steel wire containing the coating without corrosion; mount the sample according to the cross-section sample preparation method, and the sample preparation is performed according to the requirements of the scanning electron microscope sample. Use conductive inserts for hot mounting when mounting. If non-conductive inserts or cold mounting are used when mounting, then the surface should be sprayed with carbon after the sample is prepared....

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Abstract

The invention discloses a method for measuring the thickness of the coating of a steel wire. According to the method, the diameter of the steel wire containing a coating is measured according to a method of averaging multiple measurement; the inlaying of the steel wire is performed according to an arbitrary angle, so that a sectional metallographic sample is prepared; the prepared metallographic sample is arranged in a scanning electron microscope, and observation is performed; backscattering photographs are taken; the center of the elliptical steel wire section is determined; the thickness ofthe coating at any point on the section is measured; and the actual thickness of the corresponding coating can be calculate according to a proportional formula. The analysis method is simple and easyto implement, is not affected by the size of the steel wire. With the method adopted, special sample preparation methods are not required; special testing equipment is not required; more accurate test results can be provided; and the measurement requirements of the thickness of the coating of the steel wire can be satisfied.

Description

Technical field [0001] The invention belongs to the field of material microstructure inspection methods, and particularly relates to a method for measuring the thickness of steel wire coating by using a scanning electron microscope. Background technique [0002] Traditional coating testing methods include non-destructive testing methods and destructive testing methods. Common non-destructive testing methods include magnetic thickness gauges, eddy current thickness gauges, ultrasonic thickness gauges, micrometer thickness gauges and X-ray spectroscopy, etc.; damage There are metallographic method and coulomb method for detection of sex. The non-destructive testing method has certain special requirements for the material of the substrate and the coating, and the detection result has a larger error compared with the destructive testing; the metallographic method needs to ensure that the prepared cross-sectional sample is perpendicular to the coating to be tested. This requirement is...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01B15/02G01B5/08
CPCG01B5/08G01B15/02
Inventor 金传伟张珂吴园园胡显军
Owner INST OF RES OF IRON & STEEL JIANGSU PROVINCE
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