Optimizing Method of Polarization Parameters of Two-electrode Clark Type Micro Dissolved Oxygen Sensor
A dissolved oxygen sensor and polarization parameter technology, applied in instruments, measuring devices, scientific instruments, etc., can solve the problems of poor detection accuracy and stability of dissolved oxygen, and achieve the effect of improving detection accuracy and stability
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Embodiment 1
[0047] Establish the functional relationship between the polarization potential E(t, t') and the polarization reaction time t and the time t' when the dissolved oxygen concentration on both sides of the oxygen permeable membrane reaches equilibrium;
[0048]
[0049] According to formula (1), in the chemical reaction, each particle in the electrolyte participates in the reaction and consumes water molecules at the same time, so the concentration of each particle changes continuously with the increase of electrolysis time t.
[0050] From the formula (1), the sensor is in the same detection environment, and the size of the polarization potential E changes with the increase of the sensor energization time t, at this time is a constant value;
[0051] In different detection environments of the sensor, the size of the polarization potential also changes with the increase of the electrolysis time t, but in the process of environment conversion, The value of will change with t...
Embodiment 2
[0060] Establish the reduction reaction rate of the trace dissolved oxygen sensor and the ratio relational expression of the oxidation reaction rate, as follows:
[0061]
[0062] In formula (2), there are:
[0063]
[0064] According to formula (3), it can be seen that the oxidation reaction rate of the anode is related to the content of silver in the anode c Ag It is related, that is, the oxidation reaction rate of the anode is related to the surface area of the anode in contact with the electrolyte, and the relationship is nonlinear. Therefore, when the mathematical relationship in formula (2) is not equal to 1, the sensor is unstable, and it is necessary to change the effective surface area of the two electrodes in contact with the electrolyte to adjust the reaction rate of the cathode and the anode, so that the mathematical relationship is equal to 1 , to ensure the balance of the ion flow, so that a stable output current can be detected in the detection of the...
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