Salt-free printing and dyeing additive applied to blend fiber and preparation method of additive
A technology of blended fibers and printing and dyeing auxiliaries, which is applied in dyeing, textiles and papermaking, and can solve problems such as environmental damage, fiber-to-fiber color difference, and achieve environmental protection and good coloring effects
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[0024] Example 1:
[0025] A preparation method of salt-free printing and dyeing auxiliaries applied to blended fibers, comprising the following steps:
[0026] A, at room temperature, add water in the reactor, set the rotating speed to 350rpm, add ethylene glycol monobutyl ether, and stir for 22min;
[0027] B, then add sodium carboxymethyl cellulose and polyoxyethylene alkyl phenol ether, stir 12min;
[0028] C. Finally raise the temperature to 68°C, adjust the rotational speed to 280rpm, add monoalkyl phosphate and rhamnose, and stir at a constant temperature for 32min;
[0029] The salt-free printing and dyeing auxiliaries for blended fibers are composed of the following components by weight: ethylene glycol monobutyl ether 24%, sodium carboxymethyl cellulose 8%, alkyl monoalkyl phosphate 7%, Rhamnose 13%, polyoxyethylene alkyl phenol ether 5% and water balance;
[0030] The structural formula (I) of the described alkyl phosphoric acid monoalkyl ester is as follows:
...
Example Embodiment
[0033] Example 2:
[0034] A preparation method of salt-free printing and dyeing auxiliaries applied to blended fibers, comprising the following steps:
[0035] A, at room temperature, add water in the reaction kettle, set the rotating speed to 400rpm, add ethylene glycol monobutyl ether, and stir for 15min;
[0036] B, then add sodium carboxymethyl cellulose and polyoxyethylene alkyl phenol ether, stir for 15min;
[0037] C. Finally raise the temperature to 60°C, adjust the rotational speed to 300rpm, add monoalkyl phosphate and rhamnose, and stir at a constant temperature for 30min;
[0038] The salt-free printing and dyeing auxiliaries applied to blended fibers are composed of the following components by weight: ethylene glycol monobutyl ether 30%, sodium carboxymethyl cellulose 6%, alkyl monoalkyl phosphate 8%, Rhamnose 8%, polyoxyethylene alkyl phenol ether 6% and water balance.
[0039] The structural formula (I) of the described alkyl phosphoric acid monoalkyl ester ...
Example Embodiment
[0042] Example 3:
[0043] A preparation method of salt-free printing and dyeing auxiliaries applied to blended fibers, comprising the following steps:
[0044] A, at room temperature, add water in the reactor, set the rotating speed to 300rpm, add ethylene glycol monobutyl ether, and stir for 25min;
[0045] B, then add sodium carboxymethyl cellulose and polyoxyethylene alkyl phenol ether, stir for 8min;
[0046] C. Finally raise the temperature to 70°C, adjust the rotational speed to 250rpm, add monoalkyl phosphate and rhamnose, and stir at a constant temperature for 40min;
[0047] The salt-free printing and dyeing auxiliaries for blended fibers are composed of the following components by weight: 20% of ethylene glycol monobutyl ether, 10% of sodium carboxymethyl cellulose, 4% of alkyl monoalkyl phosphate, Rhamnose 15%, polyoxyethylene alkyl phenol ether 3% and water balance.
[0048] The structural formula (I) of the described alkyl phosphoric acid monoalkyl ester is as...
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