A kind of thixotropic two-component silicone rubber foam sealant, preparation method and application thereof
A silicone rubber, two-component technology, used in adhesives, chemical instruments and methods, other chemical processes, etc., can solve the problems of low production efficiency, high viscosity of rubber, and decreased elasticity of sealing materials.
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[0041] The present invention also provides a preparation method of a thixotropic two-component silicone rubber foam sealant, which is characterized in that it comprises the following steps:
[0042] (1) Weigh 100 parts of bulk silicone rubber, 0.5-5 parts of foaming agent, 1-5 parts of thixotropic agent, and 15-35 parts of flame retardant according to the mass parts of component A. Mix and stir for 60-90min at -150°C and vacuum degree of 0.095~0.099Mpa to make base material a;
[0043] (2) Let the base material a stand still, and after the base material a returns to 20-25°C, add 0.25~2 parts of catalyst to the base material a, stir and mix for 30 minutes at 20-25°C and vacuum degree of 0.095~0.099MPa -60min, make A component;
[0044] (3) Weigh 100 parts of liquid silicone rubber according to the mass of component B, add 15-25 parts of reinforcing agent into a planetary mixer, and mix and stir for 60- 90min, make base material b;
[0045] (4) Let base material b stand still...
Embodiment 1
[0050] (1) A thixotropic two-component silicone rubber foam sealant, including A component and B component, A component and B component are mixed according to the mass ratio of A:B=0.5:1; the A component Parts by weight include: 100 parts of liquid silicone rubber, 5 parts of foaming agent, 5 parts of thixotropic agent, 35 parts of flame retardant, and 0.25 parts of catalyst; the B component includes by weight: 100 parts of liquid silicone rubber, 25 parts of reinforcing agent, 5 parts of crosslinking agent, 0.5 parts of inhibitor.
[0051] (2) A thixotropic two-component silicone rubber foam sealing material, the preparation process of which is:
[0052] ① Weigh 100 parts of bulk silicone rubber, 5 parts of foaming agent, 5 parts of thixotropic agent and 35 parts of flame retardant according to the mass parts of component A. Stir for 90min to make base material a;
[0053] ②Let the base material a stand still, and after the base material a returns to 20°C, add 0.25 parts of...
Embodiment 2
[0058] (1) A thixotropic two-component silicone rubber foam sealant, including A component and B component, A component and B component are mixed according to the mass ratio of A:B=1:1; the A component Parts by weight include: 100 parts of liquid silicone rubber, 3 parts of foaming agent, 3 parts of thixotropic agent, 25 parts of flame retardant, and 0.5 parts of catalyst; the B component includes by weight: 100 parts of liquid silicone rubber, 20 parts of reinforcing agent, 3 parts of crosslinking agent, and 1 part of inhibitor.
[0059] (2) A thixotropic two-component silicone rubber foam sealing material, the preparation process of which is:
[0060] ① Weigh 100 parts of bulk silicone rubber, 3 parts of foaming agent, 3 parts of thixotropic agent, and 25 parts of flame retardant according to the mass parts of component A. Stir for 60 minutes to make base material a;
[0061] ②Let the base material a stand still, after the base material a returns to 23°C, add 0.5 part of c...
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