Manufacturing method of shale cylindrical sample

A preparation method and sample technology, applied in the field of preparation of shale cylindrical samples, can solve the problems of cumbersome methods, fragmentation, and difficulty in shale drilling, and achieve the effects of simple operation and short preparation period

Inactive Publication Date: 2019-12-17
CHINA PETROLEUM & CHEM CORP +1
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  • Claims
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AI Technical Summary

Problems solved by technology

[0002] Shale cylindrical samples are an important basis and prerequisite for determining petrophysical parameters (such as porosity and permeability) in shale, but because shale is easily broken, it is very difficult to successfully drill cylindrical samples in shale, which affects the Accurate detection of shale physical parameters
[0003] At present, the drilling of rock cylinder samples is carried out according to the conventional rock cylinder drilling instrument in the presence of water. Since the shale bedding is relatively developed and easy to break, it is more likely to break due to water absorption and swelling when it encounters water. The method is more difficult for shale drilling
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Method used

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  • Manufacturing method of shale cylindrical sample

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Embodiment

[0045] In October 2016, the present invention began to be used in Sinopec Wuxi Institute of Petroleum Geology. The shale samples that are difficult to drill by conventional methods have successfully drilled shale cylinders through this method. Ratio and porosity) analysis lays the foundation.

[0046] In summary, the beneficial effects of the present invention are: there is no need to drill cylindrical samples in water, and there is no need to pour concrete outside the original state, which greatly improves the success rate of shale cylindrical sample preparation and avoids polluting rock samples. Effective analysis of shale petrophysical parameters (such as porosity, permeability, etc.) lays a solid foundation. In addition, the invention has the advantages of short preparation cycle, simple operation and the like.

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Abstract

The invention provides a manufacturing method of a shale cylindrical sample. The manufacturing method comprises the following steps: step 1, wrapping a shale sample with a plastic film; step 2, mixinggypsum powder with water to make a lacteal product; step 3, putting the shale sample wrapped by the plastic into the lacteal gypsum slurry; step 4, after solidification of the gypsum slurry, seamlessly integrating the gypsum slurry and the shale sample into a whole; step 5, performing cylindrical drilling on the shale in the absence of water; and step 6, taking out the cylindrical sample. According to the method, because cylindrical sample drilling in water and concrete pouring outside original sample are not required, the success rate of preparation of the shale cylindrical sample is greatlyimproved and the rock sample is prevented from being polluted, thereby laying the solid foundation for the effective analysis of subsequent shale rock physical property parameters (such as porosity and permeability). In addition, the method has the advantages of short preparation period, simple operation and the like.

Description

technical field [0001] The invention belongs to the field of petroleum geology, and in particular relates to a method for preparing a shale cylinder sample. Background technique [0002] Shale cylindrical samples are an important basis and prerequisite for determining petrophysical parameters (such as porosity and permeability) in shale, but because shale is easily broken, it is very difficult to successfully drill cylindrical samples in shale, which affects the Accurate detection of shale physical parameters. [0003] At present, the drilling of rock cylinder samples is carried out according to the conventional rock cylinder drilling instrument in the presence of water. Since the shale bedding is relatively developed and easy to break, it is more likely to break due to water absorption and swelling when it encounters water. This method is more difficult for shale drilling. Search related technologies through the State Intellectual Property Office. The search formula is "s...

Claims

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Application Information

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IPC IPC(8): G01N1/28
CPCG01N1/286
Inventor 谢小敏黎茂稳腾格尔李志明芮晓庆
Owner CHINA PETROLEUM & CHEM CORP
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