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Method for preparing ligustrum lucidum biological activated charcoal

A technology of chastity seed biology and activated carbon, which is applied in chemical instruments and methods, carbon compounds, inorganic chemistry, etc., can solve the problems of reducing the purity and performance of activated carbon, increasing the cost of exhaust gas treatment, and affecting the application of activated carbon, so as to achieve excellent adsorption performance and reduce Governance cost, accurate and reliable effect of the model

Active Publication Date: 2019-12-20
HENAN INST OF SCI & TECH
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the production process of activated carbon, the raw materials will bring a large amount of metal oxides and inorganic salts, which are the main components of activated carbon ash, which can reduce the purity and performance of activated carbon, so pickling and impurity removal are usually carried out in the conventional activated carbon production process, but The acid-washed activated carbon is usually acidic, and most of the industrial waste gas is usually acidic, so the existing activated carbon has low adsorption efficiency in the adsorption of industrial waste gas, which increases the cost of waste gas treatment, which in turn affects the role of activated carbon in the treatment of industrial waste gas. application

Method used

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  • Method for preparing ligustrum lucidum biological activated charcoal
  • Method for preparing ligustrum lucidum biological activated charcoal
  • Method for preparing ligustrum lucidum biological activated charcoal

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Experimental program
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Embodiment Construction

[0036] Response surface methodology to optimize experimental design and methods

[0037] Using zinc chloride as the activator for the preparation of activated carbon, three main conditions were explored, namely, the impregnation ratio, activation temperature, and activation time.

[0038] Table 1 Orthogonal test and level

[0039]

[0040] In the case of selecting the three factors of impregnation ratio, activation temperature and activation time, according to the principle of the combination of response surface method and Box-Behnken design, the orthogonal test method is used to analyze the data using Design-Expert 8.0.6 design software The analysis of processing and regression equations designed 17 sets of experiments, of which 5 sets of central experiments, and finally selected the best preparation process. The response surface test element level is shown in Table 1.

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Abstract

The invention discloses a method for preparing ligustrum lucidum biological activated charcoal. According to the method, three factors, i.e., dipping ratio, activation temperature and activation timeof an independent variable, i.e., zinc chloride, yield of a dependent variable, i.e., activated charcoal and a sulfur dioxide adsorption mathematical model are subjected to regressive analysis by using experimental design software Design-Expert, and an obtained mathematical model is good in fitting property and is accurate and reliable; an experimental result is predicted by replacing an experimental real point with the model, and optimal processing conditions for preparing the activated charcoal through burnetizing ligustrum lucidum are predicted; meanwhile, by adopting a special impurity washing mode, the defect of the conventional activated charcoal production processes that the activated charcoal is acidified due to acid pickling is overcome, and active metal ingredients in the activated charcoal are reserved; and the prepared activated charcoal is particularly applicable to adsorption of acid pickling industrial waste gases, the efficiency of adsorption is high, the waste gas treatment cost is reduced, and then, the application of the activated charcoal in the aspect of treatment of the industrial waste gases is extended.

Description

Technical field [0001] The invention belongs to the field of activated carbon preparation, and specifically relates to a method for preparing Ligustrum lucidum biological activated carbon through zinc chloride impregnation. Background technique [0002] Ligustrum lucidum, sugar cane, reed bamboo, coconut husk, etc. can all be processed to prepare activated carbon. Ligustrum lucidum is widely grown in southwestern, southern China and areas south of the Yangtze River. Shaanxi and Gansu also have large-scale cultivation. , Indonesia and other countries also have cultivation. Under normal circumstances, Ligustrum lucidum, the fruit produced by Ligustrum lucidum, is an important medicinal material in traditional Chinese medicine treatment, used to treat dizziness, early white hair and other diseases. Ligustrum lucidum contains a lot of substances, such as oleanolic acid, mannic acid, and gluconic acid. Ligustrum lucidum, as a kind of medicinal material, has the effects of strengthen...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B32/348C01B32/324
CPCC01B32/324C01B32/348
Inventor 段凌瑶李芸玲侯超逸娄慧慧邓绍新夏克东侯振雨
Owner HENAN INST OF SCI & TECH
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