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Heat treatment method for improving comprehensive performance of alloy plate

A heat treatment method and technology for alloy plates, applied in the field of heat treatment of alloys, can solve the problems affecting the development and application of alloys, low density alloys, plasticity, fracture toughness, deterioration of corrosion properties, etc. Simple and feasible effect of performance and process

Active Publication Date: 2019-12-20
AVIC BEIJING INST OF AERONAUTICAL MATERIALS
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] With the continuous development of high reliability and high weight reduction requirements in the aerospace field, alloys with lower density and higher strength are required, and the existing alloys are not competent in terms of strength level (500MPa) and density
In order to achieve this goal, moderately increase the content of some alloying elements, increase the degree of solid solution saturation of the alloy to obtain an alloy with higher strength and lower density. In the process of thermal deformation, it is easy to precipitate a large number of needle-like "Widmanstite (Al 2 CuLi, T 1 phase)” organization, the structure has a strong “hereditary” nature, which is difficult to eliminate in the subsequent solid solution and aging process, thus deteriorating the performance of plasticity, fracture toughness, corrosion and other aspects, affecting the subsequent development and development of the alloy. application
[0003] Therefore, it is necessary to provide a technical solution for the problem that the "Widmansterite" structure in high-alloy content alloy products is difficult to eliminate, which affects the overall performance, to meet the needs of the existing technology

Method used

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  • Heat treatment method for improving comprehensive performance of alloy plate
  • Heat treatment method for improving comprehensive performance of alloy plate
  • Heat treatment method for improving comprehensive performance of alloy plate

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Experimental program
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Effect test

Embodiment 1

[0035] Using the method for improving the overall properties of the alloy involved in the present invention, the alloy composition and weight percentage are: Cu3.8%, Li 1.61%, Mg 0.38%, Zn 0.42%, Mn 0.38%, Zr 0.10%, Ti 0.06%, Si0.06%, Fe 0.08%, the balance is Al, a hot-rolled plate sample with a thickness of 80mm (high-magnification metallographic structure such as figure 1 shown), then solution quenching at 530°C for 8h, water quenching at room temperature) + pre-stretching with a deformation of 4.6% + double-stage artificial aging treatment (125°C / 20h+145°C / 10h) and solution quenching (530°C / 8h, water quenching at room temperature) + spheroidizing aging (240°C / 16h) + second (or repeated) solution quenching (530°C / 4h, water quenching at room temperature) + pre-stretching (pre-stretching deformation 4.6%) + double-stage artificial aging treatment (125°C / 20h+145°C / 10h), respectively measure the tensile, fracture properties, intergranular, spalling and stress corrosion resistanc...

Embodiment 2

[0041] Adopting the method for improving the overall performance of the alloy involved in the present invention, the alloy composition and weight percentage are: Cu4.5%, Li 1.8%, Mg 0.46%, Ag 0.35%, Zn 0.20%, Mn 0.38%, Zr 0.08%, Ti 0.03%, Si0.06%, Fe 0.08%, the balance is Al, and the free forgings with a thickness of 100mm are respectively solution quenched (535℃ / 10h, room temperature water quenching) + cold deformation (compression deformation 5.0%) + Two-stage artificial aging treatment (120℃ / 20h+148℃ / 14h) and solution quenching (535℃ / 10h, water quenching at room temperature) + spheroidizing aging (260℃ / 20h) + secondary solution quenching (535℃ / 5h, room temperature water quenching) + cold deformation (compression deformation 5.0%) + double-stage artificial aging treatment (120℃ / 20h+148℃ / 14h). After the completion, the tensile, fracture properties, intergranular, peeling and stress corrosion resistance (C ring) of the forgings were measured respectively. The results are show...

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Abstract

The invention provides a heat treatment method for improving the comprehensive performance of alloy. The alloy contains the following components of, by weight, 3.5%-4.5% of Cu, 1.4%-1.80% of Li, 0.2%-0.8% of Mg, 0.2%-0.8% of Zn, 0.04%-0.20% of Zr, 0.20%-0.80% of Mn, any one to three kinds of 0.05%-0.35% of Sc, 0.2%-0.8% of Ag and 0.10%-0.25% of Er, less than or equal to 0.08% of Si, less than or equal to 0.10% of Fe, less than or equal to 0.10% of Ti, less than or equal to 0.05% of other impurities individually, less than or equal to 0.15% of the other impurities in total, and the balance Al.The method comprises the following steps that after the alloy is subjected to solid solution and quenching, "spheroidizing aging" treatment is performed for 10 hours to 20 hours at 220 DEG C to 280 DEG C, the micron-scale granular precipitated phase is formed in the crystal, meanwhile, the large-size flake-and-needle-like "Widmanstatten structure" remained at the crystal boundary is converted intothe intermittent granular equilibrium phase, then repeated solid solution treatment, cold deformation treatment and aging treatment are performed, so that re-dissolution of the micron-scale granularprecipitated phase is achieved, moreover, precipitation of the nano-scale precipitated phase is promoted, the characteristic tissue with the uniform and tiny in-crystal precipitated phase and the intermittently-distributed crystal boundary precipitated phase is obtained, then the comprehensive performance of the alloy is improved, and the method is suitable for alloy thick plates, forge pieces andlarge-section extrusion materials used in the fields of aviation and weapons.

Description

technical field [0001] The invention relates to a heat treatment technology for alloys, in particular to a heat treatment method for improving the comprehensive properties of alloy plates. Background technique [0002] With the continuous development of high reliability and high weight reduction requirements in the aerospace field, alloys with lower density and higher strength are required, and the existing alloys are not competent in terms of strength level (500MPa) and density. In order to achieve this goal, moderately increase the content of some alloying elements, increase the degree of solid solution saturation of the alloy to obtain an alloy with higher strength and lower density. In the process of thermal deformation, it is easy to precipitate a large number of needle-like "Widmanstite (Al 2 CuLi, T 1 phase)” organization, the structure has a strong “hereditary” nature, which is difficult to eliminate in the subsequent solid solution and aging process, thus deterior...

Claims

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Application Information

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IPC IPC(8): C22F1/057C22C21/16C22C21/18
CPCC22C21/16C22C21/18C22F1/057
Inventor 李国爱吴秀亮郝敏陆政王建国
Owner AVIC BEIJING INST OF AERONAUTICAL MATERIALS
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