Oligochitosan and preparation method thereof
A technology of oligochitooligosaccharides and shrimp and crab shells, which is applied in the field of oligosaccharides, can solve the problems of reducing production efficiency, increasing production processes, and increasing production costs, and achieves the goals of improving production efficiency, reducing preparation processes, and reducing labor costs. Effect
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Embodiment 1
[0023] Embodiment 1: A kind of oligomeric chitosan, comprising the following raw materials in parts by weight: 50 parts of shrimp and crab shells, 20 parts of hydrochloric acid, 5 parts of concentrated sulfuric acid, 4 parts of nitric acid, 5 parts of nitric acid, 10 parts of sodium hydroxide solution and 30 parts organic solution.
[0024] Preferably, the mass concentration of sodium hydroxide is 5%.
[0025] Preferably, the organic solvent is methanol or ethanol.
[0026] Another technical problem to be solved in the present invention is to provide a kind of preparation method of chitosan oligosaccharide, comprising the following steps:
[0027] 1) Put 50 parts of shrimp and crab shells into the cleaning machine to clean them, remove excess impurities, then break the cleaned shrimp and crab shells into small pieces, and use a grinder to grind the broken shrimp and crab shells into small pieces Grinding, the grinding time is 10-20min, to obtain decalcified shrimp and crab s...
Embodiment 2
[0033] Embodiment 2: A kind of oligomeric chitosan, comprising the following raw materials in parts by weight: 50 parts of shrimp and crab shells, 30 parts of hydrochloric acid, 7 parts of concentrated sulfuric acid, 5 parts of nitric acid, 8 parts of nitric acid, 20 parts of sodium hydroxide solution and 50 parts organic solution.
[0034] Preferably, the mass concentration of the sodium hydroxide is 5%.
[0035] Preferably, the organic solvent is methanol or ethanol.
[0036] Another technical problem to be solved in the present invention is to provide a kind of preparation method of chitosan oligosaccharide, comprising the following steps:
[0037] 1) Put 50 parts of shrimp and crab shells into the cleaning machine to clean them, remove excess impurities, then break the cleaned shrimp and crab shells into small pieces, and use a grinder to grind the broken shrimp and crab shells into small pieces Grinding, the grinding time is 10-20min, to obtain decalcified shrimp and cr...
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