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Industrialization method of oxygen pressure acid leaching of primary uranium molybdenum ore

A technology of oxygen pressure acid leaching and molybdenum ore, which is applied in the field of oxygen pressure acid leaching of primary uranium and molybdenum ore, can solve the problems of low resource utilization rate, low molybdenum leaching rate, and high environmental risk, so as to improve resource utilization rate and improve leaching The effect of high efficiency and safety performance

Active Publication Date: 2021-09-17
中核沽源铀业有限责任公司
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Problems solved by technology

[0005] The purpose of the present invention is to solve the problems of the existing uranium and molybdenum leaching process, such as poor adaptability to changes in mineral properties, low molybdenum leaching rate, low resource utilization rate, large potential environmental risk, and high cost, to propose an industrialized method for leaching primary uranium and molybdenum ore

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  • Industrialization method of oxygen pressure acid leaching of primary uranium molybdenum ore

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Embodiment Construction

[0024] Below in conjunction with embodiment the present invention is further introduced:

[0025] An industrial method for oxygen pressure acid leaching of primary uranium molybdenum ore, comprising the following steps:

[0026] Step 1. Grinding, grading, and pulping the uranium-molybdenum symbiotic raw ore to obtain an ore pulp with a solid content of 30%-42% and a particle size of -100 mesh ≥ 95%;

[0027] Step 2, add 92.5% - 98% concentration of sulfuric acid pre-soaking in the pulp; use the recovered steam to preheat to 80 - 90 ℃;

[0028] Step 3. The preheated pulp is continuously sent into the horizontal pressurized reactor through the pulp pump. In the first stage of the horizontal pressurized reactor, it is continuously stirred and directly heated to above 140°C with steam, and oxygen is introduced at the same time. , Control the pressure of the reactor to 0.6--0.95MPa, and the second stage of the reactor starts to stabilize the temperature at 160--180°C. Reactor oxy...

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Abstract

The invention belongs to the technical field of oxygen pressure acid leaching of primary uranium and molybdenum ores, and specifically relates to a method for the existing uranium and molybdenum leaching process, which has poor adaptability to mineral property changes, low molybdenum leaching rate, low resource utilization rate, large potential environmental risk and high cost. Problem, the proposed industrialized method for leaching primary uranium and molybdenum ore; including the following steps: Step 1, grinding, grading, and pulping uranium and molybdenum symbiotic raw ore; Step 2, adding 92.5%-98% concentration of sulfuric acid to the pulp for pre-leaching ; Use the recovered steam to preheat to 80-90°C; Step 3, the preheated slurry is continuously sent into the horizontal pressurized reactor through the slurry pump, and the first stage of the horizontal pressurized reactor is continuously stirred , continuously obtain leached pulp; step 4, the obtained leached pulp is recovered steam through flash evaporation equipment for preheating raw pulp. The temperature of the pulp is lowered to below 110°C; step 5, the pulp is further heat-exchanged with the washing cold water, through solid-liquid separation, the slag is removed to the tailings pond, and the filtrate enters the next process.

Description

technical field [0001] The invention belongs to the technical field of oxygen pressure acid leaching of primary uranium and molybdenum ores, and in particular relates to an industrialized method for oxygen pressure acid leaching of primary uranium and molybdenum ores. Background technique [0002] my country's molybdenum resources are very rich, but most of them belong to complex and polymetallic associated ores that are difficult to select. Using the conventional stirring leaching method, the leaching recovery rate is very low, and the waste of resources is serious. Uranium-molybdenum paragenetic ore has high economic value, but because some ores have poor ore-forming properties, low grade, and high degree of oxidation of molybdenum, it is difficult to enrich the useful metals by using traditional physical or chemical beneficiation techniques. Due to the complex existence of forms, in addition to molybdenum minerals such as molybdenum, iron molybdenum, molybdenum calcium o...

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22B3/08C22B34/34C22B60/02
CPCC22B3/08C22B34/34C22B60/0234
Inventor 李映兵任志刚万俊刘永涛霍玉宝高东星袁征李平金凤博
Owner 中核沽源铀业有限责任公司
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