Novel high-temperature-resistant hot inlay material
A new type of high temperature resistant technology, applied in the field of metallographic sample inlays, can solve the problem that the thermal deformation temperature cannot meet the experimental requirements, and achieve the effect of low cost, high strength and good wear resistance
Inactive Publication Date: 2020-02-04
HARBIN UNIV OF SCI & TECH
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Problems solved by technology
It has the characteristics of high wear resistance, excellent chemical stability and dimensional stability, but the disadvantage is that the thermal deformation temperature cannot meet the experimental requirements
Method used
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Embodiment approach 1
[0022] The following components are included in parts by mass: 5 parts of mixed liquor, 14 parts of aluminate cement and 3 parts of water.
Embodiment approach 2
[0024] The following components are included in parts by mass: 5 parts of mixed liquid, 14 parts of aluminate cement, and 3.5 parts of water.
Embodiment approach 3
[0026] The following components are included in parts by mass: 5 parts of mixed liquor, 14 parts of aluminate cement and 4 parts of water.
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Abstract
The invention relates to a novel hot inlay material for inlaying of a metallographic sample and relates to composition design and a curing process of a novel hot inlay material. The hot inlay materialconsists of a mixed liquid, aluminate cement and water. The inlay material consists of the following components in parts by mass: 4-5 parts of the mixed liquid, 13-16 parts of the aluminate cement and 1.5-4 parts of the water. The mixed liquid consists of the following components in parts by mass: 1 part of methyl hexahydrophthalic anhydride, 1 part of methyl nadic anhydride, and 3 parts of an epoxy resin. The curing process is carried out for 24-48 hours at 150-160 DEG C. The hot inlay material prepared according to the formula and the curing process is good in forming, high in hardness, high in strength, good in wear resistance, high in deformation resistance at a high temperature, and still hard and non-deformation at 300 DEG C, and in addition, the operation is easy, the cost is low and environmental friendliness is achieved.
Description
technical field [0001] The invention relates to the field of metallographic sample inlay materials, and has the characteristics of high deformation resistance at high temperature, low cost and convenient operation. Background technique [0002] The invention aims to solve the problem that the inlaid material softens during the experiments of electron microscopy and mechanical properties of the micro-sample inlaid at high temperature (≤300° C.). [0003] Inlaid metallographic sample preparation has three functions, the sample is fixed for the adjustment of the observation surface; the sample support is used to support the observation surface during grinding and polishing; the standardized shape is used for easy clamping during grinding and polishing. The hardness and strength of the mounting material remain basically unchanged at high temperature is the prerequisite for electron microscopy and mechanical properties at high temperature. [0004] Thermal mounting material is c...
Claims
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IPC IPC(8): C04B28/06
CPCC04B28/06C04B22/002C04B24/281C04B24/04
Inventor 孙凤莲韩帮耀庞树帅刘洋
Owner HARBIN UNIV OF SCI & TECH
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