Method for rapidly determining content of mercaptoacetic acid

A technology for rapid determination of thioglycolic acid, which is applied in chemical analysis by titration, measuring device, and material analysis by observing the influence of chemical indicators. The effect of low adaptability and equipment requirements
CN111007197AInactive Publication Date: 2020-04-14中检科健(天津)检验检测有限责任公司

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
中检科健(天津)检验检测有限责任公司
Publication Date
2020-04-14
Estimated Expiration
Not applicable · inactive patent

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Abstract

The invention provides a method for rapidly determining the content of mercaptoacetic acid. The method comprises the following steps: oxidizing sulfydryl by iodine under an alkaline condition; limiting the reaction speed through IO3<->generated by reaction; and determining the titration end point to obtain the content of mercaptoacetic acid. According to the method for rapidly determining the content of mercaptoacetic acid, the recovery rate of a mercaptoacetic acid titration method reaches 98%; meanwhile, the method is stable.
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Description

technical field

[0001] The invention belongs to the field of cosmetics, in particular to a rapid determination method for thioglycolic acid content. Background technique

[0002] Thioglycolic acid is the main raw material of daily cosmetic cold perm essence and depilatory agent. The content determination method under 3.9 Thioglycolic acid in Cosmetics Technical Specifications (2015 Edition) is high performance liquid chromatography, ion chromatography and titration. Thioglycolic acid has strong acidity, and requires a very low pH value to achieve better chromatographic behavior under reversed-phase chromatography conditions. Too low pH can reduce column life and increase detection cost. Ion chromatography requires the support of less widespread ion chromatographs. The third analysis method is titration with iodine titration solution in acidic environment. In comparison, the third method is economical and simple, and is very suitable for the determination of the content o...

Claims

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