Fiber anti-sliding agent and preparation method thereof
An anti-slip agent and fiber technology, applied in the direction of fiber treatment, wear-resistant fiber, improved hand feeling fiber, etc., can solve the problems of affecting the appearance of the fabric, being easy to be torn, shortening the service life of the fabric, etc., to improve the yarn Slip resistance and sewing strength, prevention of slipping phenomenon, effect of preventing slipping
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[0032] A kind of preparation method of fiber anti-slip agent of the present invention, comprises the following steps: 1) take polyethylene oxide, polyvinyl alcohol, pentaerythritol, isophorone diisocyanate, silica sol, imino diisocyanate Succinic acid and deionized water, standby; 2) in deionized water, add polyvinyl alcohol, polyethylene oxide, pentaerythritol, isophorone diisocyanate, silica sol and iminodisuccinic acid successively, Stir and react at 50-70°C for 1-3h; 3) Cool down to below 40°C to obtain fiber anti-slip agent.
[0033] Preferably, in the step 2), the stirring speed is 500-800r / min.
Embodiment 1
[0035] A kind of preparation method of fiber anti-slip agent of the present invention, comprises the following steps:
[0036] 1) Weigh raw materials: 3 parts of polyethylene oxide, 4 parts of polyvinyl alcohol, 5 parts of pentaerythritol, 30 parts of isophorone diisocyanate, 25 parts of silica sol, 5 parts of iminodisuccinic acid, 28 parts of deionized water, the molecular weight of polyethylene oxide is 1000, the molecular weight of polyvinyl alcohol is 15000, and the degree of alcoholysis of polyvinyl alcohol is 87%, standby;
[0037] 2) Add deionized water into the reactor equipped with thermometer, stirrer, condensing reflux tube and dropping funnel, add polyvinyl alcohol, polyethylene oxide, pentaerythritol, isophorone diisocyanate, di Silica sol and iminodisuccinic acid were stirred and reacted at 50°C for 2 hours;
[0038] 3) Cool down to 40°C, discharge the material, and obtain fiber anti-slip agent.
Embodiment 2
[0040] A kind of preparation method of fiber anti-slip agent of the present invention, comprises the following steps:
[0041] 1) Weigh raw materials: 4 parts of polyethylene oxide, 3 parts of polyvinyl alcohol, 7 parts of pentaerythritol, 35 parts of isophorone diisocyanate, 30 parts of silica sol, 6 parts of iminodisuccinic acid, 15 parts of deionized water, the molecular weight of polyethylene oxide is 4000, the molecular weight of polyvinyl alcohol is 12 000, the degree of alcoholysis of polyvinyl alcohol is 89%, pentaerythritol is monopentaerythritol, and the molecular weight of isophorone diisocyanate is The purity is 99.8%, reserve;
[0042] 2) Add deionized water into the reactor equipped with thermometer, stirrer, condensing reflux tube and dropping funnel, add polyvinyl alcohol, polyethylene oxide, pentaerythritol, isophorone diisocyanate, di Silica sol and iminodisuccinic acid were stirred at a stirring speed of 500 rpm, heated to 60°C, and reacted for 3 hours;
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