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Organic solvent saturated steam segmented spice extraction device and using method thereof

A technology of organic solvents and spices, which is applied in the field of organic solvent saturated steam segmental extraction of spices, which can solve the problem of difficult recovery and extraction of aroma

Pending Publication Date: 2020-08-18
YUNNAN YANGRUI TECH GRP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to provide a device for extracting spices by organic solvent saturated steam in stages and its use method, so as to solve the problem that the aroma in spices is not easy to recover and extract

Method used

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  • Organic solvent saturated steam segmented spice extraction device and using method thereof
  • Organic solvent saturated steam segmented spice extraction device and using method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] A device for extracting spices in stages with organic solvent saturated steam, comprising a reaction kettle 1, an electric heating jacket 2 is arranged on the side wall of the reaction kettle 1, a liquid inlet pipe 3 is connected to the bottom of the reaction kettle 1, and a control valve is arranged on the liquid inlet pipe 3 A4;

[0037] The top of the reaction kettle 1 is connected with a condensation pipe 5, and the condensation pipe 5 is provided with a pressure reducing valve 6 and a tube condenser 7. The reaction kettle 1 is connected with the spice tank 8 through the condensation pipe 5, and the bottom of the condensation pipe 5 is connected with a spray device 9;

[0038] The spraying device 9 is arranged as a zigzagging spray pipe and the side wall of the spray pipe has an outlet,

[0039] Spices are placed in the spice tank 8, and the outer wall of the spice tank 8 is provided with thermal insulation cotton 10; the reaction kettle 1 enters the solvent throug...

Embodiment 2

[0041] On the basis of Example 1, the bottom of the spice tank 8 is connected to the output pipe 11, and the output pipe 11 is provided with a coil condenser 12, and the bottom of the output pipe 11 is connected to a three-way valve 13, and the three-way valve 13 is connected to three liquid storage pipes 14 , the liquid storage pipe 14 is connected to the collection tank 15, and the bottom of the collection tank 15 is connected to the drain pipe 16, and the drain pipe 16 is provided with a control valve B28; the condensed solvent and the incompletely condensed solvent vapor are communicated through the output pipe 11 of the spice tank 8 The coil condenser 12 is used to condense again, and the condensed solvent with aroma after condensation is output through the three-way valve 13, and the aroma condensed solvent can be collected in stages according to time, steam temperature in the reaction kettle 1, etc., and collected in the collection tank 15 .

Embodiment 3

[0043]On the basis of embodiment 1-2, pressure sensor 17, temperature sensor 18 are arranged on reactor 1, and the probe of temperature sensor 18 is arranged in reactor 1, and reactor 1 top connects exhaust pipe 19, and exhaust pipe 19 is provided with a control valve C20, the pressure sensor 17, the temperature sensor 18, and the control valve C20 are all connected to the first controller 21; the pressure sensor 17 monitors the pressure in the reactor 1, and when the pressure is high, the control valve C20 is opened. To adjust the pressure of the reactor 1, the temperature sensor 18 monitors the temperature in the reactor 1, and determines whether to open the pressure reducing valve 6 according to the heating temperature.

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Abstract

The invention discloses an organic solvent saturated steam segmented spice extraction device and a using method thereof. The device comprises a reaction kettle, an electric heating sleeve is arrangedon the side wall of the reaction kettle, a liquid inlet pipe is connected to the bottom of the reaction kettle, and a control valve (A) is arranged on the liquid inlet pipe. A condenser pipe is connected to the top of the reaction kettle, a pressure reducing valve and a tubular condenser are arranged on the condenser pipe, the reaction kettle is communicated with a spice tank through the condenserpipe, and a spraying device is connected to the bottom of the condenser pipe. The spraying device is a folded spraying pipe, an outlet is formed in the side wall of the spraying pipe, spice is placedin the spice tank, and heat preservation cotton is arranged on the outer wall of the spice tank. Gas-liquid mixed extraction is carried out by adopting organic steam solvent molecular diffusion, so that the requirement of segmented extraction of components is met, and a certain separation effect is achieved.

Description

technical field [0001] The invention relates to the technical field of extracting spices, in particular to a device for extracting spices in stages with organic solvent saturated steam and a method for using the same. Background technique [0002] Spices, also known as fragrance raw materials, are substances that can be smelled or tasted by the sense of smell, and are used to prepare essences. Except for individual varieties, most spices cannot be used alone. Spices are divided into natural flavors and artificial flavors, of which natural flavors include animal natural flavors and plant natural flavors; artificial flavors include isolated flavors and synthetic flavors. [0003] Spices contain aroma, which can be extracted by solvents, and the aroma components contained in the extract are extracted in sections according to different selection conditions. The ingredients in the segmented extracts are different and can be used to make different products. Therefore, a device ...

Claims

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Application Information

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IPC IPC(8): C11B9/00
CPCC11B9/00
Inventor 邵全李友宏温光和盛光发业超段勤王段刚
Owner YUNNAN YANGRUI TECH GRP
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