Composite electrolyte, preparation method thereof, and composite electrode sheet and battery comprising same
A composite electrolyte and electrode pole piece technology, which is applied in the manufacture of electrolyte batteries, non-aqueous electrolyte batteries, non-aqueous electrolyte battery electrodes, etc., can solve the problem that the impedance of the electrolyte and the pole piece has not been solved well, and achieve a lower interface Impedance, improve ionic conductivity, and avoid short circuit effects
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Embodiment 1
[0098] This embodiment provides a composite electrolyte, which includes a composite layer and a polymer layer; the composite layer includes a PVDF-LLZTO porous solid electrolyte layer with a porosity of 80%, an average pore diameter of 15.7 μm, and a thickness of 20 μm, and PMMA-based gel electrolyte filled in the pores of the porous solid electrolyte layer, the pores include interpenetrating pores and pores distributed on the surfaces of both sides of the porous solid electrolyte; the polymer layer is a 18 μm thick PEO-based polymer solid electrolyte layer.
[0099] The preparation method of composite electrolyte described in this embodiment comprises the following steps:
[0100] (1) Preparation of porous layer
[0101] Calculate the porosity and pore-forming dose of the porous layer according to the amount of gel electrolyte added, and the mass parts are 70 parts of LLZTO, 30 parts of PVDF, and 30 parts of LiN(SO 2 CF 3 ) 2 Mix with 25 parts of pore-forming agent ammoni...
Embodiment 2
[0108] This embodiment provides a composite electrolyte, which includes a composite layer and a polymer layer; the composite layer is a PVDF-LLZTO porous solid electrolyte layer with a porosity of 40%, an average pore diameter of 8.4 μm, and a thickness of 25 μm, and PMMA-based gel electrolyte filled in the pores of the porous solid electrolyte layer, the pores include interpenetrating pores and pores distributed on the surfaces of both sides of the porous solid electrolyte; the polymer layer is a 15 μm thick PEO-based polymer solid electrolyte layer.
[0109] The preparation method of the composite electrolyte described in this example is carried out with reference to the method in Example 1.
Embodiment 3
[0111] This embodiment provides a composite electrolyte, which includes a composite layer and a polymer layer; the composite layer is a PVDF-LLZTO porous solid electrolyte layer with a porosity of 60%, an average pore diameter of 12.1 μm, and a thickness of 18 μm, and PMMA-based gel electrolyte filled in the pores of the porous solid electrolyte layer, the pores include interpenetrating pores and pores distributed on the surfaces of both sides of the porous solid electrolyte; the polymer layer is a 10 μm thick PEO-based polymer solid electrolyte layer.
[0112] The preparation method of the composite electrolyte described in this example is carried out with reference to the method in Example 1.
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Abstract
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