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Ash column preparation device and method

A preparation device and ashing technology, applied in the field of carbonaceous material conversion, can solve problems such as high sealing requirements and unstable pressure, and achieve the effects of wide application range, convenient operation and simple equipment

Pending Publication Date: 2020-12-29
HEZE UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the air pressure method is mostly used in the preparation of the ash column. The air pressure method has high requirements on the sealing of the equipment, otherwise the pressure will be unstable.

Method used

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  • Ash column preparation device and method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Example 1: Preparation of 10MPa Wheat Straw Ash Column

[0033] Specific steps are as follows:

[0034] (1) Wheat straw samples were crushed to between 0.018-025mm, and made into ash at 575°C according to ASTM E1755-1 standard;

[0035] (2) Put about 1 gram of ash into the porcelain boat, add 0.08g / mL dextrin water suspension, mix well and make the coal ash reach the level that can be bonded by pressing with a knife;

[0036] (3) Put a round tube with an inner diameter of 5mm on the outside of the support rod, and add the wet ash into the round tube;

[0037] (4) Insert the stage and the pressure rod into the round tube filled with ash;

[0038] (5) According to the diameter of the round tube, the mass of the stage and pressure rod, and the pressure required for the ash column, the mass of the required weight is 5kg;

[0039] (6) Place a 5kg weight on the stage, and after 10 minutes of static pressure, remove the weight, stage and pressure bar;

[0040] (7) Slowly r...

Embodiment 2

[0042] Embodiment 2: the preparation of mixed ash column

[0043] Specific steps are as follows:

[0044] (1) Rice straw samples and coal ash were mixed at a ratio of 2:1, crushed to a size between 0.020-025mm, and made into ash at 575°C according to ASTM E1755-1 standard;

[0045] (2) Put about 1.5 grams of ash into the porcelain boat, add 0.1g / mL dextrin water suspension, mix well and make the coal ash reach the level that can be bonded by pressing with a knife;

[0046] (3) Put a round tube with an inner diameter of 8.0mm on the outside of the support rod, and add the wet ash into the round tube;

[0047] (4) Insert the stage and the pressure rod into the round tube filled with ash;

[0048] (5) According to the diameter of the circular tube, the mass of the stage and the pressure rod, and the pressure required for the ash column, the mass of the required weight is 7kg;

[0049] (6) Place a 7kg weight on the stage, and after 20 minutes of static pressure, remove the weig...

Embodiment 3

[0052] Embodiment 3: the preparation of mixed ash column

[0053] Specific steps are as follows:

[0054] (1) Corn straw samples, wheat straw samples and fly ash were mixed at a mass ratio of 1.5:1:1, crushed to a size between 0.020-025mm, and made into ash at 575°C according to the ASTM E1755-1 standard;

[0055] (2) Put about 2 grams of ash into the porcelain boat, add 0.15g / mL dextrin water suspension, mix well and make the coal ash reach the level that can be bonded by pressing with a knife;

[0056] (3) Put a round tube with an inner diameter of 10.0mm on the outside of the support rod, and add the wet ash into the round tube;

[0057] (4) Insert the stage and the pressure rod into the round tube filled with ash;

[0058] (5) According to the diameter of the round tube, the mass of the stage and the pressure rod, and the pressure required for the ash column, the mass of the required weight is 15kg;

[0059] (6) Place a 15lg weight on the stage, and after 5 minutes of s...

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Abstract

The invention relates to the technical field of conversion of carbon-containing substances such as coal and biomass, in particular to an ash column preparation device and method. The ash column preparation device is composed of a support, an objective table, a pressure rod, a circular pipe, a supporting rod and weights with different masses, wherein the supporting rod is fixed to the support. Whenan ash column is prepared, weights with different masses are added to the objective table to control the preparation pressure of the ash column. The equipment for preparing the coal and biomass carbon-containing substance ash column under the certain pressure is simple, convenient to operate, high in pressure control accuracy and wide in application range, and has obvious advantages in the aspectof preparing the ash column under the certain pressure to measure the sintering melting characteristic of ash.

Description

[0001] (1) Technical field [0002] The invention relates to the technical field of conversion of carbonaceous substances such as coal and biomass, in particular to an ash column preparation device and method. [0003] (2) Background technology [0004] Ash sintering and melting flow characteristics are important indicators for the clean conversion (combustion and gasification) of carbonaceous substances such as coal and biomass. During the conversion process, due to the inadaptability of the ash fusion characteristics of coal and other carbonaceous substances, the efficiency will drop, slagging and equipment corrosion will even lead to the shutdown of the entire conversion system. In order to determine the operating temperature for the conversion of carbonaceous substances such as coal and biomass and to accurately control the ash fusion characteristics of carbonaceous substances such as coal and biomass, the accurate determination of the ash fusion temperature of carbonaceous...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/28
CPCG01N1/286
Inventor 李风海李洋樊红莉郭明晰徐美玲赵超越
Owner HEZE UNIV
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