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Construction method of electrochemical sensor for rapidly and quantitatively detecting pesticide residues

A technology for pesticide residue detection and construction methods, applied in the direction of material electrochemical variables, scientific instruments, instruments, etc., to achieve low-cost effects

Active Publication Date: 2020-12-29
河北地质大学
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  • Abstract
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  • Claims
  • Application Information

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Problems solved by technology

[0005] In order to solve the above-mentioned technical problems, the present invention provides a method for constructing an electrochemical sensor for rapid quantitative detection of pesticide residues, which solves the shortcomings of various existing methyl parathion detection technologies, and has low detection limits, fast and accurate detection, Easy to carry, less equipment required, low cost, etc.

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  • Construction method of electrochemical sensor for rapidly and quantitatively detecting pesticide residues
  • Construction method of electrochemical sensor for rapidly and quantitatively detecting pesticide residues

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Embodiment Construction

[0036] The specification and claims do not use the difference in name as a way to distinguish components, but use the difference in function of components as a criterion for distinguishing. As mentioned throughout the specification and claims, "comprising" is an open term, so it should be interpreted as "including but not limited to". "Approximately" means that within an acceptable error range, those skilled in the art can solve the technical problem within a certain error range and basically achieve the technical effect.

[0037] The orientation terms such as up, down, left, and right in this specification and claims are combined with the drawings for further explanation, making this application easier to understand, and not limiting this application. In different scenarios, up and down, left and right, and inside and outside are all Relatively speaking.

[0038] The present invention will be described in further detail below in conjunction with the accompanying drawings.

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Abstract

The invention discloses a construction method of an electrochemical sensor for rapidly and quantitatively detecting pesticide residues, relates to the technical field of food safety detection and analysis, overcomes the defects of various existing methyl parathion detection technologies, and has the advantages of low detection limit, rapidness and accuracy in detection, convenience in carrying, less required equipment, low cost and the like. According to the specific scheme, the construction method comprises the following steps of S1, carrying out self-assembly on 4-aminothiophenol on a sulfhydrylated graphene modified silk-screen printing electrochemical sensor; S2, self-assembling methyl parathion on the sulfhydrylated graphene modified silk-screen printing electrochemical sensor; and S3, preparing a sulfhydrylated graphene loaded gold platinum nanoparticle modified molecularly imprinted silk-screen printing electrochemical sensor: preparing the methyl parathion molecularly imprintedpolymer electrochemical sensor by adopting an electro-polymerization method. The construction method of the electrochemical sensor for rapidly and quantitatively detecting pesticide residues providesa miniature pesticide residue detection chip which is rapid, sensitive, portable, low in cost and easy to operate.

Description

technical field [0001] The invention relates to the technical field of food safety detection and analysis, more specifically, it relates to a construction method of an electrochemical sensor for rapid quantitative detection of pesticide residues. Background technique [0002] At present, conventional detection methods for pesticide residues include: chromatography, spectroscopy, biochemical methods, etc. Gas chromatography, high performance liquid chromatography, and gas-mass spectrometry are widely used in laboratory testing. Although the test results are accurate, the required instruments are expensive, the sample processing and testing cycle is long, and the operation is cumbersome and time-consuming. Analysts have high technical requirements and are not suitable for on-site testing. Spectroscopic detection of organophosphorus pesticides has a limited range, background light source, low sensitivity, narrow concentration range, and poor selectivity. It is generally used a...

Claims

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Application Information

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IPC IPC(8): G01N27/30G01N27/48
CPCG01N27/308G01N27/48
Inventor 赵晶张衡李金涛魏浩吴玉会李霄刘卓常洪伦汪敬忠
Owner 河北地质大学
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