Preparation method of high-purity aluminum oxide ceramic substrate

A high-purity alumina and ceramic substrate technology, applied in the field of ceramic materials, can solve the problems of poor controllability of sintering process, poor controllability of sintering shrinkage, large forming defects of high-purity alumina ceramic substrate, etc. Good controllability, widening sintering range, small deformation effect

Pending Publication Date: 2021-01-05
SHANDONG RES & DESIGN ACADEMY OF IND CERAMICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technical effect describes various methods for producing highly purity aluminium oxide (AO). These techniques involve reducing costs while maintaining desired properties such as compact structure or better quality. They include mixing raw material together beforehand without adding any chemical agents like talcs, bauxite, silica sand, etc., creation of fine particles called alpha-aluminate crystals, drying them, cutting it down into smaller pieces, and finally subjecting the resulting fragments to heat treatment processes. Additionally, they use specialized equipment to improve production efficiency and prevent issues related to poor surface appearance and internal cracks generated when manufacturing Al2O3 ceramtic bodies.

Problems solved by technology

This patents discusses various methods that aim towards improving the quality and efficiency of producing thin films made from special materials like Aluminium oxide cerams or High Purity Aluminum Ceramics, particularly those containing rare elements called Yttrium OyAl2. These techniques include manufacturing processes based on conventional castings, powder metallurgies, plasma spray coating, electrospunning, laser ablation, thermal annealing, sol gel method, etc., but they all suffer from issues related to imperfections caused by these factors including inspexposition faults, difficulty in achieving precise dimensions, lack of effective feedback systems for dimension adjustment, and difficulties in obtaining consistently good products despite being subjected to multiple processing steps.

Method used

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  • Preparation method of high-purity aluminum oxide ceramic substrate
  • Preparation method of high-purity aluminum oxide ceramic substrate
  • Preparation method of high-purity aluminum oxide ceramic substrate

Examples

Experimental program
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Embodiment 1

[0030] A method for preparing a high-purity alumina ceramic substrate in this embodiment includes the following steps:

[0031] S1. Slurry preparation: put 99 parts by weight of high-purity alumina powder and 1 part by weight of sintering aid into a ball mill, use water as a solvent, add a water-soluble dispersant, grind and mix to obtain Ceramic slurry with high solid content, good fluidity and uniform suspension;

[0032] S2. Molding: Place the ceramic slurry in a closed container after vacuum defoaming, take the ceramic slurry corresponding to the weight required by the mold and put it into the slurry tank, add catalyst and initiator, stir evenly, and connect the slurry tank to the air Source, open the air source to apply pressure to the ceramic slurry in the slurry tank to control the ceramic slurry in the slurry tank through the connecting pipe with a control valve connecting the slurry tank and the grouting port at the bottom of the mold at a rate of 340ml / min The injec...

Embodiment 2

[0040] A method for preparing a high-purity alumina ceramic substrate in this embodiment includes the following steps:

[0041] S1. Slurry preparation: put 99.3 parts by weight of high-purity alumina powder and 0.7 parts by weight of sintering aid into a ball mill, use water as a solvent, add a water-soluble dispersant, grind and mix to obtain Ceramic slurry with high solid content, good fluidity and uniform suspension;

[0042] S2. Molding: Place the ceramic slurry in a closed container after vacuum defoaming, take the ceramic slurry corresponding to the weight required by the mold and put it into the slurry tank, add catalyst and initiator, stir evenly, and connect the slurry tank to the air Source, open the air source to apply pressure to the ceramic slurry in the slurry tank to control the ceramic slurry in the slurry tank through the connecting pipe with a control valve connecting the slurry tank and the grouting port at the bottom of the mold at a rate of 450ml / min The ...

Embodiment 3

[0050] A method for preparing a high-purity alumina ceramic substrate in this embodiment includes the following steps:

[0051] S1. Slurry preparation: put 99.5 parts by weight of high-purity alumina powder and 0.5 parts by weight of sintering aid into a ball mill, use water as a solvent, add a water-soluble dispersant, grind and mix to obtain Ceramic slurry with high solid content, good fluidity and uniform suspension;

[0052] S2. Molding: Place the ceramic slurry in a closed container after vacuum defoaming, take the ceramic slurry corresponding to the weight required by the mold and put it into the slurry tank, add catalyst and initiator, stir evenly, and connect the slurry tank to the air Source, open the air source to apply pressure to the ceramic slurry in the slurry tank to control the ceramic slurry in the slurry tank through the connecting pipe with a control valve connecting the slurry tank and the grouting port at the bottom of the mold at a rate of 580ml / min The ...

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Abstract

The invention provides a preparation method of a high-purity aluminum oxide ceramic substrate, which comprises the following steps: S1, putting 99-99.5 parts by weight of high-purity aluminum oxide powder and 0.5-1 part by weight of a sintering aid into a ball mill, adding a water-soluble dispersing agent by using water as a solvent, and grinding and mixing to obtain slurry; S2, filling the slurryinto a slurry barrel after vacuum defoaming, adding a catalyst and an initiator, uniformly stirring, connecting an air source, opening the air source to apply pressure to the slurry to control the slurry to be injected into a mold from a slurry injection port in the bottom of the mold through a communicating pipe, enabling the slurry to flow in the mold from bottom to top until the mold is filledwith the slurry, curing and demolding to obtain a green body; S3, drying the green body, softening, cutting the green body into green body slices, and drying; and S4, sintering the green body slices,and flattening to obtain the substrate. The substrate is low in sintering temperature, wide in sintering range and controllable in sintering contractibility.\ The air source is used for applying pressure to slurry, so that the slurry is injected into the mold from bottom to top from the bottom of the mold, and the problems of large blank density difference and large molding defects caused by deposition of materials with high specific gravity in the slurry to the bottom of the mold are solved.

Description

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Claims

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Application Information

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Owner SHANDONG RES & DESIGN ACADEMY OF IND CERAMICS
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