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LIBS system capable of automatically aligning and focusing

An automatic alignment and focusing mirror technology, applied in the field of spectral detection, can solve the problem that the laser cannot focus vertically to ablate the surface of the sample, and achieve the effect of improving the analysis accuracy, signal quality, and experimental accuracy and stability.

Active Publication Date: 2021-01-19
HUAZHONG UNIV OF SCI & TECH
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  • Claims
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Problems solved by technology

[0006] In view of the defects of the prior art, the purpose of the present invention is to provide a LIBS system with automatic alignment and focusing, aiming to solve the problem that the laser cannot focus vertically and ablate the surface of the sample when the LIBS technology detects samples with uneven surfaces

Method used

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  • LIBS system capable of automatically aligning and focusing
  • LIBS system capable of automatically aligning and focusing
  • LIBS system capable of automatically aligning and focusing

Examples

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Embodiment

[0061] Now take the automatic alignment and focusing of ore with uneven surface as an example to illustrate the use process of the LIBS automatic alignment and focusing detection device of the present invention. The specific operation steps are as follows:

[0062] Optical path correction of LIBS automatic alignment focusing detection device: adjust the position of the first focusing lens so that the laser focus point and the image of the surface of the sample to be tested in the area array CCD camera are most clearly at the same level.

[0063] Obtain ore surface height information: first, place the ore sample on the stage, the computer drives the five-axis electric displacement system to make the ore sample be located directly below the laser ranging sensor, and the computer controls the five-axis electric displacement system to translate, so that the laser distance measurement The sensor collects the height information of a point every x=2μm on the ore sample surface. The l...

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Abstract

The invention provides an LIBS (Laser-induced Breakdown Spectroscopy) system capable of automatically aligning and focusing, which comprises the following steps that a sample to be detected can be translated and rotated, a computer controls a five-axis electric displacement platform to move until the surface of the sample is imaged most clearly on an area array CCD (Charge Coupled Device), and laser is just focused on the surface of the sample to be detected; and the computer controls the five-axis electric displacement system to move the sample to be detected to the clewest imaging position of the surface of the sample on the area array CCD camera, so that automatic alignment and focusing are realized. According to the method, all the aligned and focused sites can be calculated by scanning once to obtain the surface height data of the to-be-detected sample and automatically focusing once, the surface of the to-be-detected sample is quickly moved to the laser focusing position when each ablation site is switched, and the laser beam is ensured to be spatially vertical to the surface of the sample. According to the invention, a sample with an uneven surface can be quickly and automatically aligned and focused, laser is focused on the surface of the sample and a laser beam is vertical to the surface of the to-be-detected sample, so that the signal quality of a spectrum is effectively improved.

Description

technical field [0001] The invention belongs to the technical field of spectrum detection, and more particularly relates to a laser-induced breakdown spectroscopy (Laser Induced Breakdown Spectroscopy, LIBS) system with automatic alignment and focus. Background technique [0002] LIBS technology is to focus high-energy pulsed laser beams on the surface of the sample to generate ablation and associated high-temperature plasma with high brightness. By collecting and analyzing the plasma radiated light and analyzing its atomic, ion and molecular spectral lines, it can be deduced The composition and content of each element in the tested sample. This technology has the advantages of simultaneous detection of multiple elements, simple or no sample preparation, real-time analysis, in-situ detection and remote detection, etc. It is widely used in material processing, food safety, artwork identification, biomedicine, deep space exploration, etc. field. [0003] At present, there ar...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/71G01N21/01
CPCG01N21/01G01N21/718G01N2021/0112
Inventor 郭连波寇卫萍胡桢麟汪威良马浴阳黄伟华
Owner HUAZHONG UNIV OF SCI & TECH
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