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A kind of rubber internal release agent and preparation method thereof

An internal release agent and rubber technology, applied in the field of rubber additives, can solve problems such as sticking and affecting the appearance properties of rubber products, and achieve the effect of good appearance quality and good internal lubrication and flow performance.

Active Publication Date: 2022-07-01
ZHEJIANG WEIXIANG TECH GRP CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The publication number is that CN104693813A discloses a kind of fatty acid zinc soap rubber internal release agent in the patent application document, comprises stearic acid, zinc compound, stearic acid amide, paraffin and diethylene glycol ether; The problem of the mold, but it will cause slight adhesion during the demoulding process, which will affect the appearance of the rubber product

Method used

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  • A kind of rubber internal release agent and preparation method thereof
  • A kind of rubber internal release agent and preparation method thereof
  • A kind of rubber internal release agent and preparation method thereof

Examples

Experimental program
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preparation example Construction

[0032] A preparation method of a rubber internal mold release agent, comprising the following steps:

[0033] 1) Preparation of matrix component A: stearic acid, zinc compound, stearic acid amide and paraffin are respectively weighed according to their parts by weight; stearic acid is added to the reactor, heated and melted, and continuously stirred; then add The zinc compound is continued to be stirred; then the stearic acid amide and the paraffin are added in turn, and the stirring is continued to obtain a clear and translucent matrix component A;

[0034] 2) Preparation of modified component B: the modifier is added to the solvent, and then heated to 60-70 ° C, so that the modifier is completely dissolved; then add nano-calcium carbonate and emulsifier, and continue to stir until the dispersion is uniform. Active nano calcium carbonate emulsion, this is modified component B;

[0035] 3) Mix the matrix component A and the modified component B to prepare the rubber internal ...

experiment example

[0053] Use the rubber internal mold release agent prepared in Example 1 to Example 10 and Comparative Example 1 to Comparative Example 6 to be added to the rubber compound for use, and the addition amount is the rubber internal mold release agent: The rubber compound is 1: 100; Made into rubber strips, according to GB / T12829-2006, the strips were subjected to a tear strength test to judge their hot tear strength performance; the test results are shown in Table 3: Among them, Comparative Example 7 is the existing Rubber products normally used in technology;

[0054] Table 3 embodiment and the demoulding effect statistics table of comparative example

[0055]

[0056]

[0057] It can be seen from the experimental data in Table 3 that the rubber internal mold release agent of the present invention can be used in the rubber compound, which can effectively improve the tear strength of the rubber compound, thereby enhancing the hot tear strength performance of the rubber compo...

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Abstract

The invention provides an internal rubber mold release agent and a preparation method thereof. The internal rubber mold release agent is composed of a matrix component A and a modified component B in a mass ratio of 1:(0.4-0.6); the matrix Component A includes 40-65 parts of stearic acid, 10-30 parts of zinc compounds, 35-45 parts of stearic acid amides, and 9-15 parts of paraffin wax; the modified component B is composed of a weight ratio of 1:1:( 0.4-0.6): (0.5-0.7) nano calcium carbonate, solvent, modifier and emulsifier are prepared. The matrix component A and the modified component B in the rubber internal mold release agent of the present invention can improve the fluidity of the rubber material and make its internal lubricating flow performance good; the surface of the prepared rubber product has self-cleaning properties. It is easy to demould and separate the rubber product from the mold, and ensures that the surface of the rubber product after demolding is smooth and complete, and the appearance quality is good.

Description

technical field [0001] The invention belongs to the field of rubber auxiliaries, in particular to an internal rubber release agent and a preparation method thereof. Background technique [0002] The release agent is a functional substance between the mold and the rubber product. Its function is to prevent the rubber product from sticking to the mold, causing serious appearance defects of the rubber product and preventing the pollution of the vulcanized mold. The release agent can help the rubber products to be removed from the mold smoothly, ensure the appearance of the products is qualified, reduce the loss of waste products, and improve the production efficiency and economic benefits. [0003] There are two kinds of mold release agents, one is external spray type, which is directly sprayed on the vulcanized mold. Due to the use of powder as a carrier, the workshop environment is polluted seriously and the cost is high; one is a mold release agent for rubber, which is dire...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L91/06C08K13/02C08K5/09C08K3/26C08K3/22
CPCC08K13/02C08K5/09C08K3/26C08K3/22C08K2201/011C08K2003/265C08K2003/2296C08L91/06
Inventor 张立王廷山戴圣佳陶莉
Owner ZHEJIANG WEIXIANG TECH GRP CO LTD